Synthesis of Bi-Pr-O Composite Nanoflakes with Good Electrochemical Performance
نویسندگان
چکیده
Bi-Pr-O composite nanoflakes were synthesized with the aid of polyvinyl pyrrolidone (PVP) as surfactant. The characterization was performed by X-ray diffraction and electron microscopy. prepared consisted tetragonal Bi2O3, hexagonal Pr2O3, Bi0.4Pr0.6O1.5 smooth surface. size whole is less than 1 μm thickness 100 nm. formation can be explained a PVP-assisted growth mechanism. A systematic study electrochemical catalysis L-cysteine using Bi-Pr-O-composite-nanoflake-modified electrode carried out. pair quasi-reversible anodic cathodic peaks are observed at −0.69 +0.02 V, respectively, on in 2 mM 0.1 M KCl solution. current response proportional to concentration range 0.001—2 detection limit 0.33 μM. In addition, display satisfactory reproducibility stability for L-cysteine.
منابع مشابه
Electrochemical characterisation of graphene nanoflakes with functionalised edges.
Graphene nanoflakes (GNF) of diameter ca. 30 nm and edge-terminated with carboxylic acid (COOH) or amide functionalities were characterised electrochemically after drop-coating onto a boron-doped diamond (BDD) electrode. In the presence of the outer-sphere redox probe ferrocenemethanol there was no discernible difference in electrochemical response between the clean BDD and GNF-modified electro...
متن کاملProbing the electrochemical properties of biopolymer modified EMD nanoflakes through electrodeposition for high performance alkaline batteries.
In the present work, a novel biopolymer approach has been made to electrodeposit manganese dioxide from manganese sulphate in a sulphuric acid bath containing chitosan in the absence and presence of glutaraldehyde as a cross-linking agent. Galvanostatically synthesised electrolytic manganese dioxide (EMD) nanoflakes were used as electrode materials and their electrochemical properties with the ...
متن کاملSynthesis and electrochemical performance of a polymer-derived silicon oxycarbide/boron nitride nanotube composite
Polymer-derived ceramics (PDCs) such as silicon oxycarbide (SiOC) have shown promise as electrode materials for rechargeable Li-ion batteries (LIBs) owing to the synergy between their disordered carbon phase and hybrid bonds of silicon with oxygen and carbon. This study describes the synthesis and characterization of a new type of PDC composite comprising SiOC embedded with varying wt% of boron...
متن کاملsingle-step synthesis of multi-component spirobarbiturates using ionic liquids and synthesis of substituted pyridine filled with catalysts supported on solid substrate
in this thesis, a better reaction conditions for the synthesis of spirobarbiturates catalyzed by task-specific ionic liquid (2-hydroxy-n-(2-hydroxyethyl)-n,n-dimethylethanaminium formate), calcium hypochlorite ca(ocl)2 or n-bromosuccinimide (nbs) in the presence of water at room temperature by ultrasonic technique is provided. the design and synthesis of spirocycles is a challenging task becaus...
15 صفحه اولذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: E-journal of Surface Science and Nanotechnology
سال: 2023
ISSN: ['1348-0391']
DOI: https://doi.org/10.1380/ejssnt.2023-049