Studi Sintesis, Karakterisasi, dan Sifat Magnetik Senyawa Kompleks Nikel-N,N’-Dietiltiourea klorida
نویسندگان
چکیده
Senyawa kompleks dari garam nikel dengan ligan N,N’ -dietiltiourea ( detu ) perbandingan mol 1:4 berhasil disintesis dan dikarakterisasi metode reaksi langsung refluks. Kompleks Ni- (DR) Ni-detu(R) yang secara berurutan refluks mempunyai titik lebur 159-161°C 114-116°C. Analisis data FT-IR kedua sampel menunjukkan ikatan υ(N-H) Ni-detu berada pada rentang 3233-3235 cm -1 , υ(C-H) 2964-2974 υ(C-N) 1562-1579 υ(C=S) 646-653 . refinement XRD diperoleh Rwp sebesar 11,63% senyawa terbentuk kemiripan struktur [Ni( 4 ]Cl 2 Hasil pengukuran VSM hasil sintesis (R) menujukkan keduanya bersifat diamagnetik.
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ژورنال
عنوان ژورنال: JC-T (Journal Cis-Trans) : jurnal kimia dan terapannya
سال: 2023
ISSN: ['2549-6573', '2549-6565']
DOI: https://doi.org/10.17977/um0260v7i12023p016