Structure determination by single-crystal X-ray diffraction (SXD) at megabar pressures
نویسندگان
چکیده
منابع مشابه
Structure of sodium above 100 GPa by single-crystal x-ray diffraction.
At pressures above a megabar (100 GPa), sodium crystallizes in a number of complex crystal structures with unusually low melting temperatures, reaching as low as 300 K at 118 GPa. We have utilized this unique behavior at extreme pressures to grow a single crystal of sodium at 108 GPa, and have investigated the complex crystal structure at this pressure using high-intensity x-rays from the new D...
متن کاملThree-dimensional structure of a single colloidal crystal grain studied by coherent x-ray diffraction.
A coherent x-ray diffraction experiment was performed on an isolated colloidal crystal grain at the coherence beamline P10 at PETRA III. Using azimuthal rotation scans the three-dimensional (3D) scattered intensity from the sample in the far-field was measured. It includes several Bragg peaks as well as the coherent interference around these peaks. The analysis of the scattered intensity reveal...
متن کاملRedetermination of the crystal structure of β-zinc molybdate from single-crystal X-ray diffraction data
The crystal structure of the β-polymorph of ZnMoO4 was re-determined on the basis of single-crystal X-ray diffraction data. In comparison with previous powder X-ray diffraction studies [Katikaneani & Arunachalam (2005 ▸). Eur. J. Inorg. Chem. pp. 3080-3087; Cavalcante et al. (2013 ▸). Polyhedron, 54, 13-25], all atoms were refined with anisotropic displacement parameters, leading to a higher pr...
متن کاملEVALUATION OFDISLOCATION STRUCTURE AND CRYSTALLITE SIZE IN WORN AL-SI ALLOY BY X-RAY DIFFRACTION
Abstract: powerful method for the characterization of microstructures of crystalline materials in terms of crystallite size anddislocation structures. In this paper the effect of the sliding on the microstructure of A356 in the as-cast and heattreated conditions are studied, The X-ray phase analysis shows that with increasing applied load, the dislocationdensity is increased, whereas the crysta...
متن کاملMagnetism in FeO at Megabar Pressures from X-Ray Emission Spectroscopy
We report evidence for a preserved magnetic state in FeO up to 143 GPa at room temperature using high-resolution x-ray emission spectroscopy. This observation is based on the spectral line shape of the Fe Kb emission line. Up to the highest pressure, FeO remains a magnetic insulator. Combining our results with previous Mössbauer data, we present a new magnetic phase diagram of FeO. Features lik...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Journal of Synchrotron Radiation
سال: 2005
ISSN: 0909-0495
DOI: 10.1107/s0909049505024945