Solventless Synthesis ofN-Protected Amino Acids in a Ball Mill
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چکیده
منابع مشابه
Rapid synthesis of nucleotide pyrophosphate linkages in a ball mill.
Using a ball mill, rapid, atom-economic coupling between adenosine-5'-phosphoromorpholidate and phosphorylated ribose derivatives as their sodium or barium salts was achieved. Facile purification by reversed-phase HPLC enabled product isolation within hours.
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Large macrocycles containing imine and borasiloxane links are obtained in polycondensation reactions of 4-formylbenzeneboronic acid, t-Bu(2)Si(OH)(2), and diamines. The multicomponent reactions can be performed in solution or--advantageously--by mechanochemical syntheses in a ball mill.
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Science, a weekly journal founded in 1880, is published each Friday by the American Association for the Advancement of Science at the Business Press, 10 McGovern Ave., Lancaster, Pa. Editorial and Advertising Offices, 1515 Massachusetts Ave., N.\., Washington 5, D. C. Telephone, Executive 6060. Cable address, SCIMAG, Washington, D. C. Entered as second-class matter at the Post Office at Lancast...
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ژورنال
عنوان ژورنال: ACS Sustainable Chemistry & Engineering
سال: 2013
ISSN: 2168-0485,2168-0485
DOI: 10.1021/sc4001115