Solid Phase Extraction in Pesticides Residue Analysis
نویسندگان
چکیده
منابع مشابه
Solid-phase extraction method for the quantitative analysis of organochlorine pesticides in wildlife urine.
A gas chromatographic method for the analysis of nine organochlorine pesticides in wildlife urine is described. Reversed-phase solid-phase extraction is utilized to extract the organochlorine pesticides from urine. The pesticides are recovered by elution with hexane-ethyl ether (1:1) and quantified by gas chromatography with electron-capture detection. Method detection limits range from 1.4 to ...
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A new extraction and cleanup procedure with gas chromatography was developed for the sensitive determination of acephate, dimethoate, malathion, diazinon, quinalphos, chlorpyrifos, profenofos, alpha-endosulfan, beta-endosulfan, chlorothalonil and carbaryl using 1-chloro-4-fluorobenzene as an internal standard in fruits and vegetables. Several extracting and eluting solvents for solid-phase extr...
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In this work, the determination of a group of triazolopyrimidine sulfoanilide herbicides (cloransulam-methyl, metosulam, flumetsulam, florasulam, and diclosulam) in soy milk by capillary electrophoresis-mass spectrometry (CE-MS) is presented. The main electrospray interface (ESI) parameters (nebulizer pressure, dry gas flow rate, dry gas temperature, and composition of the sheath liquid) are op...
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Phosalone, malathion and diazinon were analyzed in corn oil using solid phase extraction (SPE)with lanthanum silicate as a new solid sorbent followed by gas chromatography with nitrogenphosphorus detection (GC-NPD). The efficiency of different eluents (methanol, dichloromethane,ethyl acetate, dichloromethane — ethyl acetate (1:1) and ethyl acetate — methanol (1:1)) werecompared for elution of o...
متن کاملMulti-Residue Confirmation of Pesticides in Honey using Solid Supported Liquid Extraction
Several Belgian beekeepers were asked to shut down their hives due to withering of the hive. The cause of the withering was unknown. A multi-factoral study was initiated, which included a multi-class pesticide residue study from honey, to determine if pesticides were the cause of the decline. The extensive distribution of pesticides causes bees that have been fed on contaminated blossoms to tra...
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ژورنال
عنوان ژورنال: Journal of Pesticide Science
سال: 2002
ISSN: 1348-589X,1349-0923
DOI: 10.1584/jpestics.27.444