Silica extract from Malang beach sand via leaching and sol-gel methods
نویسندگان
چکیده
<span>Many silica minerals are found in beach sands. One of its sands is Bajul Mati sand which contains high silica. The can be extracted using existing methods, but it less environmentally friendly. In this research, the extracting process from (South Java-Indonesia) has been carried out through a method that low-cost and more friendly</span><span lang="IN">.</span><span> purpose study was to characterize with instrumentation results economic analysis. </span><span>via leaching sol-gel methods: i) 7</span><span>M HCl</span><span lang="IN">,</span><span>ii) formation clear sodium silicate solution (Na<sub>2</sub>O.SiO<sub>2</sub>)</span><span lang="IN">,</span><span>iii) sol-gel: titrated oxalic acid (H<sub>2</sub>C<sub>2</sub>O<sub>4</sub>) 1 M until pH 6 obtained silicite Si(OH)<sub>4</sub> formed</span><span lang="IN">,</span><span> iv) characterization X-ray fluorescence (XRF), diffraction (XRD), Fourier transform infrared (FTIR), scanning electron microscopy (SEM) </span><span lang="IN">with</span><span> result showed cristobalite structure based on XRD purity (% Wt Si) reached 93.9% XRF FTIR analysis identified silanol, siloxic, siloxane groups. SEM shows (SiO<sub>2</sub>) particles tend form agglomerations about </span><span>∼</span><span>1 μm. lang="IN">In a</span><span>ddition, will support implementation future, so produced by developed method.</span>
منابع مشابه
Iron Oxide Silica Derived from Sol-Gel Synthesis
In this work we investigate the effect of iron oxide embedded in silica matrices as a function of Fe/Si molar ratio and sol pH. To achieve homogeneous dispersion of iron oxide particles, iron nitrate nonahydrate was dissolved in hydrogen peroxide and was mixed with tetraethyl orthosilicate and ethanol in a sol-gel synthesis method. Increasing the calcination temperature led to a reduction in su...
متن کاملCarbon–silica sol-gel derived nanomaterials
The preparation of sol-gel derived silica-based nanomaterials containing electrical conductive carbon fillers in an extensive composition range is described and their electrical properties are presented. Nanomaterials of carbon filler concentrations up to 60% (v/v) were obtained by dip coating or screen-printing from precursors of hydrolysed alkoxysilanes. Nanostructured morphology could be ide...
متن کاملA Parametric Study of the Synthesis of Silica Nanoparticles via Sol-Gel Precipitation Method
In this study, SiO2 nanoparticles were successfully synthesized via sol-gel precipitation method and the effects of different parameters such as temperature, ethanol, ammonia and tetraethylorthosilicate (TEOS) contents based on water were investigated in a systematic way applying Taguchi experimental design method. It was found that, among all the investigated parameters, ethanol as a co-solven...
متن کاملSol-gel-derived biomaterials of silica and carrageenans.
A new precursor, tetrakis(2-hydroxyethyl) orthosilicate (THEOS), introduced by Hoffmann et al. (J. Phys. Chem. B 106 (2002) 1528-1533), was used to synthesize monolithic hybrid biomaterials on the basis of silica and three main types of carrageenans, kappa-, iota-, and lambda-carrageenans. The advantage of THEOS over the currently applied TEOS and TMOS is in its complete solubility in water. Th...
متن کاملSol–Gel Synthesis and Characterization of Microporous Silica Membranes
It has been reported in the literature that the composition Unsupported silica membranes were prepared by acid-catalyzed of the synthesis solution influences the structure of the spehydrolysis and condensation of tetraethylorthosilicate. The possicies in the sol (3) and, hence, the final structure of the bility of tailoring the pore size and porosity of microporous silica membrane. This possibi...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: International Journal of Advances in Applied Sciences
سال: 2023
ISSN: ['2252-8814', '2722-2594']
DOI: https://doi.org/10.11591/ijaas.v12.i1.pp74-81