Reactions of excited-state benzophenone ketyl radical in a room-temperature ionic liquid

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Reactions of excited-state benzophenone ketyl radical in a room-temperature ionic liquid.

The photochemistry of the benzophenone ketyl radical in D(1) excited state, BPH(D(1)), was studied by means of two-color dual-pulse laser flash photolysis (355 and 532 nm) in a room-temperature ionic liquid, 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)amide (Bmim-TFSA), and in methanol. Upon excitation with the 532 nm pulse, BPH(D(1)) emitted strong fluorescence. The transient absor...

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Influence of Ionic Liquids on Physico Chemical Reactions Reactions of Excited-State Benzophenone Ketyl Radical in a Room-Temperature Ionic Liquid

The photochemistry of benzophenone ketyl radical in the D1 excited state, BPH(D1), was studied by means of two-color dual-pulse laser flash photolysis (355 and 532 nm) in a room-temperature ionic liquid, 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)amide (Bmim-TFSA), and in methanol. Upon excitation with the 532-nm pulse, BPH(D1) emitted strong fluorescence. The transient absorption ...

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Structural and spectroscopic characterization of a charge-separated uranium benzophenone ketyl radical complex.

The reaction of [((t-Bu)ArO) 3tacn)U (III)] ( 1) with 4,4'-di- tert-butylbenzophenone affords a unique isolable U(IV) ketyl radical species [((t-Bu)ArO) 3tacn)U (IV)(OC* (t-Bu)Ph 2)] (2) supported by XRD data, magnetization measurements, and DFT calculations. Isolation and full characterization of the corresponding diphenyl methoxide complex [((t-Bu)ArO) 3tacn)U (IV)(OCH ( t-Bu )Ph 2)] (3) is a...

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Isolation of a uranium(III) benzophenone ketyl radical that displays redox-active ligand behaviour.

The first uranium(III) charge separated ketyl radical complex, Tp*2U(OC·Ph2), has been isolated and characterized by infrared, (1)H NMR, and electronic absorption spectroscopies, along with X-ray crystallography. Tp*2U(OC·Ph2) is a potent two-electron reductant towards N3Mes (Mes = 2,4,6-trimethylphenyl) and (2,2,6,6-tetramethyl-piperidin-1-yl)oxyl (TEMPO), with reducing equivalents derived fro...

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ژورنال

عنوان ژورنال: Physical Chemistry Chemical Physics

سال: 2010

ISSN: 1463-9076,1463-9084

DOI: 10.1039/b920131a