Reaction of Aliphatic 1, 2-Nitro-alcohols with Semicarbazide and 2, 4-Dinitrophenylhydrazine
نویسندگان
چکیده
منابع مشابه
1-Benzoyl-4-(2-nitrophenyl)semicarbazide
The title compound, C(14)H(12)N(4)O(4), was prepared by the reaction of 2-nitro-phenyl isocyanate with benzoyl-hydrazine. The dihedral angle between the rings is 71.49 (6)) Å. The mol-ecular conformation is stabilized by an intra-molecular N-H⋯O hydrogen bond, generating an S(6) ring. The crystal packing shows N-H⋯O hydrogen bonds.
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متن کامل(E)-1-Nitro-4-(2-nitroethenyl)benzene
The asymmetric unit of the title compound, C(8)H(6)N(2)O(4), consists of two independent mol-ecules with similar geometries, each adopting a trans configuration about the olefinic double bond. The two mol-ecules are both almost planar (r.m.s. deviations = 0.034 and 0.035 Å) and form a dihedral angle of 83.62 (2)°. Short N⋯O contacts [2.834 (3)-2.861 (3) Å] are observed between the nitro groups ...
متن کاملN-(2-Chloro-2-nitro-1-phenylpropyl)-4-methylbenzenesulfonamide
In the title compound, C(16)H(17)ClN(2)O(4)S, the dihedral angle between the phenyl and benzene rings is 19.4 (2)°. The crystal packing is stabilized by inter-molecular N-H⋯O hydrogen bonds, as well as by intra- and inter-molecular C-H⋯O hydrogen bonds.
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ژورنال
عنوان ژورنال: Nippon kagaku zassi
سال: 1960
ISSN: 0369-5387,2185-0917
DOI: 10.1246/nikkashi1948.81.5_804