Multivariate Curve Resolution for 2D Solid-State NMR spectra
نویسندگان
چکیده
منابع مشابه
Improving the quality of 2D solid-state NMR spectra of microcrystalline proteins by covariance analysis.
Gaining time, resolution and sensitivity at the same time: covariance processing of two-dimensional NMR spectra of microcrystalline proteins improves spectral quality over conventional Fourier transformation despite a significant reduction of the experimental time.
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Article history: Received 16 January 2008 In final form 15 May 2008 Available online 21 May 2008 0009-2614/$ see front matter 2008 Elsevier B.V. A doi:10.1016/j.cplett.2008.05.045 * Corresponding author. Fax: +972 8 9344123. E-mail address: [email protected] (L Few analytical techniques rival the capabilities of two-dimensional nuclear magnetic resonance. A scheme enabling 2D NMR acq...
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MOTIVATION When analyzing solid-state nuclear magnetic resonance (NMR) spectra of proteins, assignment of resonances to nuclei and derivation of restraints for 3D structure calculations are challenging and time-consuming processes. Simulated spectra that have been calculated based on, for example, chemical shift predictions and structural models can be of considerable help. Existing solutions a...
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ژورنال
عنوان ژورنال: Analytical Chemistry
سال: 2020
ISSN: 0003-2700,1520-6882
DOI: 10.1021/acs.analchem.9b05420