Monoclinic superstructure of mullite-type KAl9O14
نویسندگان
چکیده
منابع مشابه
Superstructure of Mullite-type KAl9O14
Large whiskers of a new KAl9O14 polymorph with mullite-type structure were synthesized. The chemical composition of the crystals was confirmed by energy-dispersive X-ray spectroscopy, and the structure was determined using single-crystal X-ray diffraction. Nanosized twin domains and one-dimensional diffuse scattering were observed utilizing transmission electron microscopy. The compound crystal...
متن کاملTricalcium silicate Ca 30 [ Si 04 J : The monoclinic superstructure
Crystals, free from twinning, ofthe monoclinic phase oftricalcium silicate exhibiting superstructure reflections have been obtained. Crystal data are: a = 33.083(8), b = 7.027(2), e = 18.499(4) A, f3 = 94.12(2)°, Z = 36 x CaZ.89Mgo.ll0Si04, V = 4289 A3. The structure analysis was carried out using 3886 independent reflection intensities measured on a single-crystal diffractometer. The unit cell...
متن کاملNanocomposite mullite/mullite powders by spray pyrolysis
A mullite/mullite nanocomposite powder has been synthesized, composed of nanometer-size 3Al2O3 · 2SiO2 (‘3 : 2’) mullite precipitates within a matrix of the high alumina 2Al2O3 · SiO2 (‘2 : 1’) mullite. Historically, the transition from the metastable high-alumina phase to the thermodynamically stable ‘3 : 2’ phase of mullite has been thought to be a continuous process, involving a continuous s...
متن کاملMicrowave Sintering of Mullite
Microwave sintering possesses unique attributes and has the potential to be development as a new technique for controlling microstructure and to improve the properties of advanced ceramics. Because microwave radiation penetrates most ceramics, uniform volumetric heating is possible. Thermal gradients, which are produced during conventional sintering because of conductive and radioactive heat tr...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Acta Crystallographica Section A Foundations of Crystallography
سال: 2010
ISSN: 0108-7673
DOI: 10.1107/s0108767310096078