Measurement of Outgassing Rate from Stainless Steel Chamber for Ultra High Vacuum and Extreme High Vacuum.

A Road Map to Extreme High Vacuum

Ultimate pressure of a well-designed vacuum system very much depends on pretreatments, processing and procedures [1, 2]. Until now much attention has been paid to minimizing hydrogen outgassing from the vacuum chamber wall materials, however, procedures and processing deserve further scrutiny. For reducing the gas load, high sensitivity helium leak detection techniques with sensitivities better...

Rolling Contact Fatigue in Ultra High Vacuum

Constructing an Ultra-High Vacuum Chamber and a Radio Frequency Helical Resonator for Trapping Ions

We describe the construction of an ultra-high vacuum (UHV) chamber and a radio frequency helical resonator for use in co-trapping atomic and molecular ions. Cleaning procedures for the in-vacuum components are provided. These procedures give positive results in cleaning copper electrodes. The thesis also provides general UHV construction techniques and design choices for our UHV chamber. For th...

Vacuum Brazing of Zirconium-Based Alloy and 321 Stainless Steel Using Titanium Based Filler Metal

Both Zirconium-based alloys and 321stainless steel are widely used as engineering alloys due to their good mechanical properties. Conventional fusion welding techniques for Zr alloys and stainless steel are not feasible due to the formation of brittle intermetallic compounds such as (Zr3Fe, ZrFe2 and Zr2Fe) and corrosion cracking. Brazing is one of the most wide...

Selective Hydrogenation of Acetylene over Palladium in Ultra High Vacuum

Under ultra-high-vacuum conditions, precoverage of a palladium(ll1) surface with hydrogen does not affect either the kinetics or the extent of acetylene uptake at 175 K. The subsequent reactive behavior of the system is however radically altered. Benzene formation is strongly suppressed, the transformation of adsorbed acetylene to another species (@-phase) is enhanced, and the yield of ethylene...