Marking Porcelain and Silica Crucibles, etc.

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Unsuitability of porcelain crucibles for dry ashing of biological tissues for calcium analysis.

At temperatures required for complete release of calcium from beef liver by dry ashing, porcelain crucibles release significant amounts of calcium into the ash, which leads to erroneously high calcium values in the samples. Heated, empty porcelain crucibles do not show released calcium. Both fused silica and platinum crucibles fail to show any significant interaction with the sample. Samples dr...

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ژورنال

عنوان ژورنال: Journal of Industrial & Engineering Chemistry

سال: 1912

ISSN: 0095-9014,1943-2968

DOI: 10.1021/ie50044a006