Hydronium bis(trifluoromethanesulfonyl)amide–18-crown-6 (1/1)

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Dibenzo-18-crown-6

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Complexation of Hydronium Ion with Several Crown Ethers in Nitromethane Solution

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(18-Crown-6)(trifluoro­methane­sulfonato)­sodium

The title compound, [Na(CF(3)O(3)S)(C(12)H(24)O(6))], features a sodium cation that is coordinated by eight O atoms in an irregular hexa-gonal bipyramidal environment. The equatorial positions are occupied by the six O atoms of an 18-crown-6 ether ring. In the axial positions, there is one O atom of a trifluoro-methane-sulfonate anion and an ether O atom of a symmetry-equivalent crown ether rin...

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Methyl­ammonium tetra­fluoridoborate 18-crown-6 clathrate

In the title compound, CH(3)NH(3) (+)·BF(4) (-)·C(12)H(24)O(6), the methyl-ammonium cation makes three N-H⋯O hydrogen bonds to the 18-crown-6 mol-ecule. The -NH(3) (+) and -CH(3) groups of the cation adopt a staggered conformation. The F atoms of the tetra-fluoridoborate anion are disordered over two sets of sites in a 0.519 (11):0.481 (11) ratio. Weak C-H⋯F inter-actions occur in the crystal, ...

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4-Methyl­anilinium tetra­fluoro­borate 18-crown-6 clathrate

In the title compound, C(7)H(10)N(+)·BF(4) (-)·C(12)H(24)O(6), the proton-ated 4-methyl-anilinium cation inter-acts with 18-crown-6 forming a rotator-stator structure, (C(6)H(4)CH(3)NH(3) (+))(18-crown-6), through three bifurcated N-H⋯(O,O) hydrogen bonds between the ammonium groups of the cations (-NH(3)) and the O atoms of the crown ether mol-ecule. The BF(4) (-) anions, the methyl group and ...

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ژورنال

عنوان ژورنال: IUCrData

سال: 2020

ISSN: 2414-3146

DOI: 10.1107/s2414314620001625