Hydrofluoric Acid-Free Digestion of Organosilicon Nanoparticles for Bioanalysis by ICP-OES
نویسندگان
چکیده
A novel ICP-OES method has been developed for the determination of Si concentration, originating from polyorganophosphosilanes, in biological specimens that also contain metal ions. The is free hazardous hydrofluoric acid (HF) and involves digestion with HNO3/H2O2 prior to analysis by ICP-OES. High reproducible spike recovery was obtained controls.
منابع مشابه
Determination of Microelements in Human Milk and Infant Formula Without Digestion by ICP-OES.
The concentrations of zinc (Zn), iron (Fe) and copper (Cu) in both human milk and infant formula were determined using a new sample preparation method, by inductively coupled plasma - optical emission spectometry (ICP-OES) and flame atomic absorption spectrometry (FAAS). Human milk samples were diluted in ultrapure water. The infant formula of powder samples (suitable for an infant 1-6 months o...
متن کاملsynthesis and determination of lead (ii) sulfide nanoparticles in rat organs by icp-oes
recent studies have reported that metal sulfide nanoparticles had potential adverse effects. in this research, lead (ii) sulfide nanoparticles have been synthesized under different reaction conditions. scanning electron microscopy and x-ray diffraction were used to characterize the particle size and morphology. distribution, accumulation and toxic effects of nanoparticles on rats as a biologic...
متن کاملA Comparative Study on Mineral Contents of Soybean by Two Methods of Digestion Using ICP-OES Technique: A Risk Assessment Study
Introduction: In recent years, the contamination of food with heavy metals has received much attention. Plants can absorb metal pollutants through contaminated water, soil, and air. Materials and Methods: In the current study, accumulation of minerals in three types of soybeans was investigated by wet and dry digestion methods using ICP-OES technique. Thereafter, the metals' health risk was as...
متن کاملcontrol of the optical properties of nanoparticles by laser fields
در این پایان نامه، درهمتنیدگی بین یک سیستم نقطه کوانتومی دوگانه(مولکول نقطه کوانتومی) و میدان مورد مطالعه قرار گرفته است. از آنتروپی ون نیومن به عنوان ابزاری برای بررسی درهمتنیدگی بین اتم و میدان استفاده شده و تاثیر پارامترهای مختلف، نظیر تونل زنی(که توسط تغییر ولتاژ ایجاد می شود)، شدت میدان و نسبت دو گسیل خودبخودی بر رفتار درجه درهمتنیدگی سیستم بررسی شده اشت.با تغییر هر یک از این پارامترها، در...
15 صفحه اولNanoparticles for bioanalysis.
This review covers the emerging field of nanobiotechnology, in which nanoparticles are applied to the analysis of biomolecules. Nanoparticles can be used in a variety of bioanalytical formats, and this review discusses four classes of use. First, nanoparticles as quantitation tags, such as the optical detection of quantum dots and the electrochemical detection of metallic nanoparticles. Second,...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Micro
سال: 2023
ISSN: ['2673-8023']
DOI: https://doi.org/10.3390/micro3010019