HPLC Determination of Capsaicinoids with Cross-Linked C18 Column and Buffer-Free Eluent
نویسندگان
چکیده
منابع مشابه
HPLC analysis of carotenoids from tomatoes using cross-linked C18 column and MS detection.
This study was conducted to analyze carotenoids from tomatoes by high-performance liquid chromatography using reversed-phase C18 silica having cross-linked end-capping with diode array and mass spectrometric detection. An efficient gradient elution system was developed to achieve good and reliable separation of both major and minor carotenoids as well as their isomers. Resolution of lycopene, β...
متن کاملDetermination of two capsaicinoids in analgesic transdermal patches using RP-HPLC and UV spectroscopy
Background and objectives: At the present time, a considerable frontier in the administration of therapeutic medications is transdermal drug delivery. Methods: In this study, a rapid, precise, sensitive and selective reversed-phasehigh performance liquid chromatography (RP-HPLC) method has been evaluated, developed and validated to separate and quantitate capsa...
متن کاملPreconcentration of Pb(II) by Graphene Oxide with Covalently Linked Porphyrin Adsorbed on Surfactant Coated C18 before Determination by FAAS
A simple, highly sensitive, accurate and selective method for determination of trace amounts of Pb(II) in water samples is presented. A novel Graphene oxide with covalently linked porphyrin solid-phase extraction adsorbent was synthesized by covalently linked porphyrin onto the surfaces of graphite oxides. The stability of a chemically (GO-H2P) especially in concentrated hydrochloric acid was s...
متن کاملPreconcentration of Pb(II) by Graphene Oxide with Covalently Linked Porphyrin Adsorbed on Surfactant Coated C18 before Determination by FAAS
A simple, highly sensitive, accurate and selective method for determination of trace amounts of Pb(II) in water samples is presented. A novel Graphene oxide with covalently linked porphyrin solid-phase extraction adsorbent was synthesized by covalently linked porphyrin onto the surfaces of graphite oxides. The stability of a chemically (GO-H2P) especially in concentrated hydrochloric acid was s...
متن کاملDetermination of urinary free cortisol by HPLC.
We here report a reversed-phase HPLC method for the determination of free cortisol in human urine, using methylprednisolone as the internal standard. Before chromatography, samples were extracted with a C18 solid-phase extraction column and the steroids were separated on a LiChrospher 100 C18 column with a mobile phase of methanol/acetonitrile/water (43/3/54 by vol). Linearity, precision, and a...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Journal of Chromatographic Science
سال: 2014
ISSN: 1945-239X,0021-9665
DOI: 10.1093/chromsci/bmu030