(E)-3-Bromo-N′-(4-methoxybenzylidene)benzohydrazide methanol solvate
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چکیده
منابع مشابه
(E)-3-Bromo-N′-(4-methoxybenzylidene)benzohydrazide methanol solvate
The title compound, C(15)H(13)BrN(2)O(2)·CH(3)OH, was synthesized by the reaction of 4-methoxy-benzaldehyde with an equimolar quantity of 3-bromo-benzohydrazide in methanol. The benzohydrazide mol-ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 4.0 (2)°. The benzohydrazide and methanol mol-ecules are linked into a chain propagating along...
متن کامل(E)-N′-(5-Bromo-2-hydroxybenzylidene)-4-hydroxy-3-methoxybenzohydrazide methanol solvate
In the title compound, C(15)H(13)BrN(2)O(4)·CH(4)O, the two benzene rings form a dihedral angle of 3.2 (2)°. An intra-molecular O-H⋯N hydrogen bond is observed. In the crystal structure, mol-ecules are linked through O-H⋯O and N-H⋯O hydrogen bonds, forming a two-dimensional network parallel to (10).
متن کاملN′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
In the title hydrazone compound, C(15)H(13)BrN(2)O(3)·CH(3)OH, the methanol solvate is linked to the benzohydrazide molecule through O-H⋯N and O-H⋯O hydrogen bonds. The benzohydrazide mol-ecule adopts an E configuration about the C=N double bond. The mol-ecule is twisted, with a dihedral angle between the two substituted benzene rings of 35.7 (2)°. In the crystal structure, mol-ecules are linke...
متن کامل3-Bromo-N′-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide methanol solvate
The title compound, C(14)H(9)Br(3)N(2)O(2)·CH(4)O, was prepared by the reaction of 3,5-dibromo-2-hydroxy-benzaldehyde and 3-bromo-benzohydrazide in methanol. The asymmetric unit of the crystal consists of a Schiff base mol-ecule and a methanol mol-ecule of crystallization. The dihedral angle between the two benzene rings is 5.5 (2)°. An intra-molecular O-H⋯N hydrogen bond is observed. In the cr...
متن کامل(E)-N′-(4-Hydroxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
The title compound, C(14)H(12)N(2)O(3)·CH(4)O, consists of a Schiff base mol-ecule and a methanol mol-ecule of crystallization. The Schiff base mol-ecule is nearly planar, the dihedral angle between the planes of the two benzene rings being 7.2 (2)°. The mol-ecule exists in the trans configuration with respect to the methyl-idene unit. In the crystal structure, the Schiff base and methanol mol-...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2009
ISSN: 1600-5368
DOI: 10.1107/s1600536809030219