Determination of Fumonisins B1 and B2 in Corn by Liquid Chromatography/Mass Spectrometry with Immunoaffinity Column Cleanup: Single-Laboratory Method Validation
نویسندگان
چکیده
منابع مشابه
Determination of fumonisins B1 and B2 in corn by LC/MS with immunoaffinity column cleanup: interlaboratory study.
An interlaboratory validation study was conducted to establish the method performance characteristics of an immunoaffinity column (IAC) cleanup procedure followed by LC/MS for the determination of fumonisins B1 (FB1) and B2 (FB2) and combined FB1 + FB2 in corn. The test portion is extracted with acetonitrile-methanol-water (25 + 25 + 50). The extract is filtered, diluted with phosphate-buffered...
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ژورنال
عنوان ژورنال: Journal of AOAC INTERNATIONAL
سال: 2008
ISSN: 1060-3271,1944-7922
DOI: 10.1093/jaoac/91.3.598