Determination of 23 Organophosphorous Pesticides in Surface Water Using SPME Followed by GC-MS
نویسندگان
چکیده
منابع مشابه
GC–MS and GC–NPD Determination of Formaldehyde Dimethylhydrazone in Water Using SPME
Formaldehyde dimethylhydrazone (FADMH) is one of the important transformation products of residual rocket fuel 1,1-dimethylhydrazine (1,1-DMH). Thus, recent studies show that FADMH toxicity is comparable to that of undecomposed 1,1-DMH. In this study, a new method for quantification of FADMH in water based on solid phase microextraction (SPME) in combination with gas chromatography (GC) with ma...
متن کاملOrganophosphorous pesticides in surface water of Iran.
This research aims to evaluate the presence and distribution of pesticides in Babolrood River of Mazandaran Province in Iran. Mean diazinon levels in surface water ranged from 77.6 to 101.6 μg L(-1) with maximum level of 768.9 μg L(-1) and mean malathion levels ranged from 55.7 to 75.9 μg L(-1) with maximum level of 506.6 μg L(-1). The residues of malathion and diazinon pesticides in all of the...
متن کاملDetermination of Sub-ppb Level of Phthalates in Water by Auto-SPME and GC-MS Application
A solid-phase microextraction (SPME) method for the analysis of phthalates in water samples was developed on the CTC CombiPAL autosampler GC-MS platform. In this method, the sample preparation process was automated by using a CombiPAL autosampler, including the SPME fiber precondition, adsorption, and desorption, which improve the precision of the SPME method. The extraction temperature, extrac...
متن کاملDevelopment of an SPME-GC-MS/MS method for the determination of pesticides in rainwater: laboratory and field experiments.
A solid-phase microextraction -- coupled to a gas chromatography -- ion trap tandem mass spectrometry (SPME-GC-MS/MS) method was developed for the quantitative determination in rainwater of 8 pesticides amongst the most used in France and 3 triazines metabolites. The main factors affecting the SPME process were studied. Using a 3 mL sample, the method developed showed good linearity for concent...
متن کاملChemical Analysis of Pesticides Using GC/MS, GC/MS/MS, and LC/MS/MS
There are well over 500 registered pesticides worldwide for use in agricultural regions and new agrochemicals are introduced to the marketplace continuously. This chapter deals with the chemical analysis methods for the main pesticide chemical classes that are most frequently analyzed with gas chromatography (GC) or liquid chromatography (LC) coupled to mass spectrometry (MS). GC amenable pesti...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Journal of Chromatographic Science
سال: 2010
ISSN: 0021-9665,1945-239X
DOI: 10.1093/chromsci/48.3.183