Crystal structure of 2-(4-methoxyphenyl)-2-cyclohexene-1-one oxime, C13H15NO2

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Synthesis and Crystal Structure of 3-(4-Methoxyphenyl)-2-thioxo-2,3-dihydroquinazolin-4(1H)-one

Synthesis of the title compound from 4-methoxyaniline was accomplished in three steps. The structure was supported by spectroscopic data and unambiguously confirmed by single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21 with unit cell dimensions a = 9.9349(8), b = 6.3377(5), c = 10.5783(10) Å, β = 97.752(3)°, V = 659.97(10) Å, Z = 2.

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Synthesis, Crystal Structure and Antibacterial Evaluation of Di-μ-chlorido-bis({2-[(4-methoxyphenyl)- iminomethyl]pyridine-κ2N,N']Mercury(II)

New coordination polymer of [HgLCl2]n (1) with HgCl2 and Schiff base bidentate ligand (4-methoxyphenyl) pyridine-2yl methyleneamine (L) was prepared and structurally characterized. In the 1D network structure of 1, the mecury (II) ion adopts an HgN2Cl3 distorted square pyramid geometry. In this complex, one of the chlorine acts as bridging ligand connecting two adjacent mercury(II) ions while, ...

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Crystal structure of 3,3-dichloro-N-p-methoxyphenyl-4-(2-phenylstryl)-2-azetidinone.

3,3-Dichloro-N-p-methoxyphenyl-4-(2-phenylstryl)-2-azetidinone (C22H15Cl2NO2) was studied by X-Ray analysis, which indicated a monoclinic space group, P2(1)/c, with a = 9.619(5), b = 13.879(4), c = 14.161(5)A, beta = 100.16(3)degrees, V = 1860.8(13)A3, Z = 4, Dc = 1.414 g cm(-3), micro(Mo Kalpha) = 0.366 mm(-1) and F000 = 816. The structure was solved by direct methods and refined to R = 0.041 ...

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(E)-4-Phenyl­butan-2-one oxime

In the title compound, C(10)H(13)NO, the C-C-C-C torsion angle formed between the benzene ring and the butan-2-one oxime unit is 73.7 (2)°, with the latter lying above the plane through the benzene ring. In the crystal, inter-molecular O-H⋯N hydrogen bonds link pairs of mol-ecules into dimers, forming R(2) (2)(6) ring motifs which are stacked along the a axis.

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Crystal structure of (E)-2-hy­droxy-1,2-di­phenyl­ethan-1-one oxime

The title compound, C14H13NO2, is a commercially available material and can be used as a multidentate ligand. The mol-ecule of the asymmetric unit has an R configuration, while the corresponding S-configured mol-ecule of the racemic mixture is generated by a crystallographic centre of symmetry. Both hy-droxy groups (the H atom of the oxime group is equally disordered over two positions) are inv...

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ژورنال

عنوان ژورنال: Zeitschrift für Kristallographie - New Crystal Structures

سال: 2001

ISSN: 2197-4578,1433-7266

DOI: 10.1524/ncrs.2001.216.14.685