منابع مشابه
2-{3-Cyano-4-[2-(4-diethylamino-2-hydroxyphenyl)ethenyl]-5,5-dimethyl-2,5-dihydrofuran-2-ylidene}malononitrile acetone 0.25-solvate
In the title compound, C(22)H(22)N(4)O(2)·0.25C(3)H(6)O, the disordered acetone mol-ecule lies with partial occupancy about the 2 axis. The mol-ecule of the malononitrile derivative is essentially planar excluding the methyl groups, with the largest deviation from the mean plane through the non-H atoms being 0.1955 (13) Å. Two rotamers with different orientations of the benzene ring are observe...
متن کاملAnalgesic activity of 3-mono-substituted derivatives of dihydrofuran-2-one in experimental rodent models of pain.
Three derivatives of dihydrofuran-2-one (L-PP, L-PP1, and L-SAL) were administered by intraperitoneal injection and their analgesic activity was assayed in several models of pain. The activity of these derivatives were tested using a hot plate test, a writhing test, capsaicin- and glutamate-induced nociception, along with two models of local anesthesia, including a test for infiltration anesthe...
متن کاملThe dihydrofuran template approach to furofuran synthesis.
Flash vacuum pyrrolysis of vinyl epoxides provides cis-dihydrofuran carboxylic esters in good yields and diastereoselectivities, which, on base-promoted epimerisation afford the complementary trans series. The compounds provide a viable template for a Lewis acid promoted cyclisation to provide the 2,6-diaryl-3,7-dioxabicyclo[3.3.0]octane core found in the furofuran series of natural lignans. Th...
متن کاملPreparation and Characterization of Ti(BH4)3(THF)3 and V(BH4)2(TMEDA)2 Complexes
We have recently synthesized Ti(BH4)3(THF)3 and V(BH4)2(TMEDA)2 complexes. The reaction of TiCl3(THF)3 with NaBH4 in dry THF gave flat blue crystals, Ti(BH4)3(THF)3. The reaction of VCl3 with NaBH4 in presence of N, N, N', N'- tetramethyle...
متن کاملCopolymerization Using Lipase Catalyst
Enzymatic ring-opening copolymerization of lactones was carried out by using Pseudomonas f luorescens lipase in bulk. In the copolymerizaton of r-caprolactone (E-CL) and b-valerolactone at 60°C for 10 days a copolymer with molecular weight of 3.7 x 103 was obtained and its structure was found to be of random structure having both units from 13C NMR anlaysis. Effects of the feed ratio, the react...
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ژورنال
عنوان ژورنال: The Journal of the Society of Chemical Industry, Japan
سال: 1970
ISSN: 0023-2734,2185-0860
DOI: 10.1246/nikkashi1898.73.3_580