Benzylation of 3-(γ-Dimethylamino-propoxy)-1H-indazole in Liquid Ammonia
نویسندگان
چکیده
منابع مشابه
1-Methyl-1H-indazole-3-carboxylic acid
The asymmetric unit of the title compound, C(9)H(8)N(2)O(2), contains two mol-ecules. In the crystal structure, both mol-ecules form inversion dimers via pairs of O-H⋯O hydrogen bonds, and a C-H⋯O inter-ation is also seen.
متن کامل1-Allyl-3-chloro-5-nitro-1H-indazole
In the title compound, C10H8ClN3O2, the indazole ring system makes a dihedral angle of 7.9 (3)° with the plane through the nitro group. The allyl group is rotated out of the plane of the indazole ring system [N-N-C-C torsion angle = 104.28 (19)°]. In the crystal, mol-ecules are linked by C-H⋯O hydrogen bonds, forming zigzag chains propagating along the b-axis direction.
متن کامل3-(4-Pyridyl)-4,5-dihydro-1H-benzo[g]indazole
In the mol-ecular structure of the title compound, C(16)H(13)N(3), the cyclo-hexa-1,3-diene ring displays a screw-boat conformation and the pyridine ring is twisted by a dihedral angle of 29.13 (9)° with respect to the pyrazole ring. Mol-ecules are linked into a supra-molecular structure by N-H⋯N hydrogen bonding.
متن کامل3-Bromo-6-nitro-1-(prop-2-ynyl)-1H-indazole
In the title compound, C(10)H(6)BrN(3)O(2), the indazole fused-ring system is nearly planar (r.m.s. deviation = 0.008 Å); its nitro substituent is nearly coplanar with the fused ring [dihedral angle = 4.5 (2)°]. In the crystal, adjacent mol-ecules are linked by weak acetyl-ene-nitro C-H⋯O hydrogen bonds, generating a helical chain running along the b axis.
متن کامل1-(4-Methylphenylsulfonyl)-5,6-dinitro-1H-indazole
In the title compound, C14H10N4O6S, the indazole ring system is almost perpendicular to the tosyl ring, as indicated by the dihedral angle of 89.40 (9)° between their planes. The dihedral angles between the indazole system and the nitro groups are 57.0 (3) and 31.9 (3)°. In the crystal, mol-ecules are linked by C-H⋯O inter-actions, forming chains running along [100].
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ژورنال
عنوان ژورنال: Journal of Synthetic Organic Chemistry, Japan
سال: 1972
ISSN: 0037-9980,1883-6526
DOI: 10.5059/yukigoseikyokaishi.30.457