Analysis of Cadmium and Lead in honey: direct-determination by Graphite Furnace Atomic Absorption Spectrometry

GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY WITH MAlIlRIX MODIFICATION FOR DETERMINATION OF LEAD IN DRINKING WATER

An amoniumvanadate plus sodium molybdate mixed modifier Graphite Furnace Atomic Absorption Spectrometric method has been developed for determination of traces of lead in drinking water. The concentration of lead in the sample is obtained by direct comparison to linear working graph prepared from aqueous standards in the modifier medium, The results indicate the better performance of the pro...

Utilization of electrodeposition on a graphite probe modified with palladium in determination of lead by graphite furnace atomic absorption spectrometry in water and environmental samples

In this work a rapid and selective procedure for separation and preconcentration of lead(Pb2+) before determination by electrothermal atomic absorption spectrometry (ETAAS) wasdeveloped. The procedure is based on the electrodeposition on a graphite probe modified withpalladium. The lead was deposited from acetate buffer solution at pH 5.5. Various parameters,such as pH of solutions, deposition ...

The Analysis of Trace Elements in Honey by Flame and Graphite Furnace Atomic Absorption Spectrometry

Determination of lead in croatian wines by graphite furnace atomic absorption spectrometry.

A method has been developed for direct determination of lead in wine by graphite furnace atomic absorption spectrometry (GFAAS) with Zeeman-effect background correction. The thermal behaviour of Pb during pyrolysis and atomisation stages was investigated without matrix modifier and in the presence of Pd(NO(3))(2), Pd(NO(3))(2) + Mg(NO(3))(2) × 6H(2)O, and NH(4)H(2)PO(4) + Mg(NO(3))(2) × 6H(2)O ...

Analysis of Low Lead and Cadmium Concentrations in Soil Extracts by Graphite Furnace Atomic Absorption Spectrophotometry

An analytical procedure was derived to provide an accurate measurement of low lead (Pb) and cadmium (Cd) concentrations in soil extracts using graphite furnace atomic absorption spectrometry (GFAAS). Based on peak area measurements and with background correction, the use of 2% phosphoric acid as chemical modifier enables the GFAAS to give measurements of Pb and Cd concentration as low as 3 fLg ...