A Novel Pentachlorophenol Electrochemical Sensor Based on Nickel-Cobalt Layered Double Hydroxide Doped with Reduced Graphene Oxide Composite

نویسندگان

چکیده

A highly sensitive non-enzymatic electrochemical pentachlorophenol (5-CP) sensor was successfully fabricated employing a multi-component sensing platform made of nickel-cobalt layered double hydroxide (NiCo-LDH) supported on green organic-inorganic nanohybrid (rGO-CuO) drop-casted gold electrode (AuE). The chemical and morphological properties the as-synthesized nanostructures were investigated confirmed by infrared spectroscopy (ATR) scanning electron microscopy (SEM). measurements demonstrated that both good conductivity large active surface area hierarchical structure NiCo-LDH/rGO-CuO favor redox reaction 5-CP. In optimized procedure, we have evaluated analytical performance NiCo-LDH/rGO-CuO/AuE using cyclic voltammetry based current intensities peaks. Our findings indicate developed exhibits wide linear range from 1 to 50 μ M while limit detection estimated be 12.64 nM for Moreover, suggested 5-CP displayed an excellent stability might provide robust practical reliable in various real samples.

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ژورنال

عنوان ژورنال: ECS advances

سال: 2023

ISSN: ['2754-2734']

DOI: https://doi.org/10.1149/2754-2734/acc117