6-(4-Methoxyphenyl)-6a-nitro-6,6a,6b,7,8,9,10,12a-octahydrospiro[chromeno[3,4-a]indolizine-12,3′-indolin]-2′-one

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6a-Nitro-6-phenyl-6,6a,6b,7,8,9,10,12a-octa­hydro­spiro­[chromeno[3,4-a]indol­izine-12,3′-indolin]-2′-one

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6-(4-Meth­oxy­phen­yl)-6a-nitro-6,6a,6b,7,8,9,10,12a-octa­hydro­spiro­[chromeno[3,4-a]indolizine-12,3′-indolin]-2′-one

In the title compound, C29H27N3O5, the hydropyran ring adopts an envelope conformation with the methine C atom bearing the para-meth-oxy-benzene ring as the flap. The central pyrrolidine ring has a twist conformation on the N-C bond involving the spiro C atom. The piperidine ring adopts a chair conformation. An intra-molecular C-H⋯O contact closes an S(7) ring. In the crystal, inversion dimers ...

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6-Hydr­oxy-3-(hydroxy­imino)indolin-2-one

In the title compound, C(8)H(6)N(2)O(3), the indol-2-one system is almost planar [maximum deviation = 0.010 (3) Å]. In the crystal structure, inter-molecular N-H⋯O, O-H⋯N and O-H⋯O hydrogen bonds link the mol-ecules into a three-dimensional network. π-π contacts between the indole ring systems [centroid-centroid distances = 3.494 (1), 3.731 (1) and 3.736 (1) Å] may further stabilize the structure.

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3-(4-Hydroxy­phenyl­imino)indolin-2-one

In the title compound, C(14)H(10)N(2)O(2), the dihedral angle between the indole and benzene rings is 61.63 (4)°. In the crystal structure, centrosymmetrically related mol-ecules are linked into dimers by N-H⋯O hydrogen bonds, generating rings of graph-set motif R(2) (2)(8). The dimers are further connected into a three-dimensional network by O-H⋯O and C-H⋯O hydrogen bonds.

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2-(4-Methyl­phen­yl)-6-nitro-1,3-benzoxazole

The title compound, C14H10N2O3, is a π-conjugated mol-ecule containing a benzoxazole aromatic fused heterobicycle. The benzoxazole ring system is planar within 0.01 Å. The mol-ecule assumes an approximately flat conformation, the benzoxazole ring system forming dihedral angles of 6.52 (12) and 7.4 (3)° with the benzene ring and the nitro group, respectively. In the crystal, mol-ecules are conne...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2013

ISSN: 1600-5368

DOI: 10.1107/s1600536813015341