4-Methoxy-N,N′-diphenylbenzamidinium nitrate
نویسندگان
چکیده
منابع مشابه
3-Methoxy-4-(4-nitrobenzyloxy)benzaldehyde
In the title compound, C(15)H(13)NO(5), the vanillin group makes a dihedral angle of 4.95 (8)° with the benzene ring of the nitro-benzene group. The packing is stabilized by weak, non-classical inter-molecular C-H⋯O inter-actions which link mol-ecules into chains running along the c axis.
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A short C-N distance [1.394 (2) Å] in the title compound, C(11)H(10)N(3)O(4)S(+)·NO(3) (-), is indicative of some conjugation of the sulfonamide π electrons with those of the pyridinium ring. The crystal structure is stabilized by N-H⋯O hydrogen bonds.
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A high-performance liquid chromatographic (HPLC) assay suitable for the evaluation of 3-methoxy-4-hydroxyphenylglycol (MHPG) in 1-ml aliquots of plasma is presented. Preparatory steps include extraction into ethyl acetate and minicolumn chromatography. Recoveries are monitored with [3H]MHPG. The HPLC procedure utilizes a C18 column, isocratic elution and amperometric detection. The assay was ch...
متن کامل4-Methylbenzylammonium nitrate
In the title salt, C8H12N(+)·NO3 (-), the N atom of the 4-methyl-benzyl-ammonium cation is displaced by 1.366 (2) Å from the mean plane of the other atoms. In the crystal, the cations are connected to the anions by N-H⋯O and N-H⋯(O,O) hydrogen bonds, generating a layered network parallel to (100). A weak C-H⋯O inter-action also occurs.
متن کامل4-Methylanilinium nitrate
The asymmetric unit of the title compound, C(7)H(10)N(+)·NO(3) (-), consists of a 4-methyl-anilinium cation protonated at the amino group and a nitrate anion. In the crystal, anions and cations are linked through N-H⋯O and N-H⋯(O,O) hydrogen bonds, buiding a corrugated layer structure parallel to (001).
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ژورنال
عنوان ژورنال: IUCrData
سال: 2016
ISSN: 2414-3146
DOI: 10.1107/s2414314616013924