the composite powders of barium-magnesium ferrite were prepared using sol-gel auto-combustion and microwave methods. the crystal structure and the shape of nanocomposites have been compared. x-ray diffraction (xrd), scanning electron microscope (sem) and vibrating sample magnetometer (vsm) were used to investigate the structural, morphological and magnetic properties of nanopowder. the formatio...

nanocrystalline particles of barium hexaferrite has been prepared by the sol–gel auto- combustion method using iron and barium nitrate with a ba:fe molar ratio of 1:10. the effect of fuel such as citric acid and aspartic acid was investigated on the structure and magnetic properties of nanoparticles. the results revealed that the formation of barium hexaferritefine particles is influenced by mo...

zro2 nanopowder was prepared by the sol-gel auto-combustion method. the product was characterized by x-ray diffraction (xrd), energy dispersive analysis of x-ray (edx) and scanning electron microscopy (sem). the average crystalline size of zro2 was obtained 62 nm. also, photocatalytic removal of nitrophenol from aqueous solution by using nanoscale zro2 under uv light irradiation was studied. th...

zno and zro2 photo catalysts were synthesized by sol-gel auto combustion method. the products were characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem). structural and morphological properties of nano particles were investigated and the average crystalline size of zno and zro2 was obtained 44 and 51 nm, respectively. also, photo catalytic degradation of nitro phenol f...

Magnetic powder of Sr-ferrite was prepared by conventional and sol-gel auto-combustion methods. In conventional method, strontium carbonate and ferric oxide powders were mixed together and then mixture was calcined. In sol-gel auto-combustion method, a solution containing strontium nitrate, ferric nitrate and citric acid was heated until the combustion took place automatically; then, as-burnt p...

sol–gel auto-combustion is a unique combination of the combustion and the chemical gelation processes. in this work, nanosize (d) powders with compositions of znfe2o4 were synthesized by sol–gel combustion method. the puffy, porous brown powders as-combusted was calcined at the temperature of 750–1000◦c for 4 h. these powders are characterized by x-ray diffraction and scanning electron microsco...

nanocrystalline complex oxides have been synthesized by combination of sol–gel auto combustion and ultrasonic irradiation techniques using copper nitrate, zinc nitrate as metallic nitrates and glycine, urea and thiourea as fuels. sol-gel combustion (combination of the chemical sol–gel process and the combustion process) as a proper synthesized technique is used to synthesize zno/cuo nanocomposi...

the dried nitrate-urea gels exhibit the combination of autoicatatric combustion behavior and ultrasonic, whichcan be used to synthesize the nanocatalyst ferrite powders. cu and ni unites nanocatalyst powders sithcomposition of caned], and nife204 were synthesized by a sol-gel auto catalnic combustion process. themolar ratio between metal ions and urea was 11.2. the sob gel process was done at 8...

nanocrystalline zro2 with particle size of about 38 nm was directly synthesized by sol-gel auto-combustion method. the overall process involved three steps: formation of homogeneous sol at 50-55°c; formation of dried gel at 110°c, and combustion of the dried gel at 400°c. experiments revealed that zro2 dried gel derived from glycine (fuel) and nitrate sol exhibited self propagating combustion a...

the cunica nanopanicles have been synthesized by sol-gel auto-combusson. microwave and co-precipitationtechniques. then, the results of the three techniques were compared. in the vol-ael auto-combustion synthesiswas used glycine as a fuel. at first, sol was prepared. then, gel was achieved from drying so'. the prepared gelwas burnt at 350°c. in the noicrowavc technique, gel was prepared. then, ...