five new aromatic poly(amide-imide)s (5a-e) were synthesized by direct polycondensationreaction of n-(4-carboxy phenyl) trimellitimide (3) with five aromatic diamines (4a-e) by usingtriphenyl phosphite in n-methyl-2-pyrrolidone (nmp) and pyridine at solution containingdissolved cacl2. all of the polymers were obtained in quantitative yields with inherentviscosities between 0.29-0.40 dl/g. the r...

The esterification reaction of trimellitic anhydride chloride TMAC 1 with N-(hydroxymethyl) phthalimide NHMP 2, N-(2-hydroxyethyl) phthalimide NHEP 3 or N-(hydroxymethyl) thalidomide NHMT 4 afforded novel cyclic imide-ester derivatives; phthaloyl-phthalic anhydride methyl ester PPAME 5, phthaloyl-phthalic anhydride ethyl ester PPAEE 6 and thalidomide-phthalic anhydride methyl ester TPAME 7, res...

Five new aromatic poly(amide-imide)s (5a-e) were synthesized by direct polycondensationreaction of N-(4-carboxy phenyl) trimellitimide (3) with five aromatic diamines (4a-e) by usingtriphenyl phosphite in N-methyl-2-pyrrolidone (NMP) and pyridine at solution containingdissolved CaCl2. All of the polymers were obtained in quantitative yields with inherentviscosities between 0.29-0.40 dL/g. The r...

This study sought to investigate the degradation mechanism of 4-methacryloyloxy ethyl trimellitic acid, 4-MET, which is commonly used as an acidic monomer in solvated self-etching primers or one-step bonding agents. To this end, we examined the effects of solvent type used--such as ethanol, methanol, and acetone--on the degradation mechanism of 4-MET by using the 13C NMR technique. The degradat...

We report a panel of carboxylates and sulfonamides incorporating phthalic anhydride and phthalimide moieties in their structure and their interaction with the metalloenzyme carbonic anhydrase (CA, EC 4.2.1.1). They were synthesized from substituted anthranilic acids and trimellitic anhydride chloride, followed by reaction with primary amines and were tested for the inhibition of five physiologi...

This study aimed to examine the shear bond strength between cobalt chromium alloy and autopolymerizing acrylic resin using experimental primers containing 5, 10, and 15 wt% of 4-methacryloxyethyl trimellitic anhydride or 1, 2, and 3 wt% of 3-methacryloxypropyl-trimethoxysilane comparison to 5 commercial primers (ML primers, Alloy primer, Metal/Zirconia primer, Monobond S, and Monobond plus). Si...

Industrial exposure to gases and fumes may produce a wide variety of respiratory damage including tracheobronchial inflammation and parenchymal damage.' Tracheobronchial inflammation is reported, particularly after exposure to chlorine, ammonia, and sulphur dioxide. Interstitial pneumonitis has been associated with the inhalation of oxides of nitrogen,2 cadmium,3 manganese,4 mercury,5 and resin...