In this work, mechanical alloying was employed to produce Ti-50Al and Ti-45Al-5Cr (at%) alloys. Alloying was performed in a planetary mill and the alloying time varying from 5 to 70h. Characterization of the powder mixture was performed by X-ray diffraction (XRD), SEM analyses and DTA test, during mechanical alloying and after annealing at 1100°c in vacuum oven. The results showed, after 50h of...