the cunica nanopanicles have been synthesized by sol-gel auto-combusson. microwave and co-precipitationtechniques. then, the results of the three techniques were compared. in the vol-ael auto-combustion synthesiswas used glycine as a fuel. at first, sol was prepared. then, gel was achieved from drying so'. the prepared gelwas burnt at 350°c. in the noicrowavc technique, gel was prepared. then, ...

in this paper, indium tin oxide (ito) nanoparticles has been prepared by chemical methods under given conditions with solution of indium chloride (incl3·4h2o), tin chloride (sncl4·5h2o) in ammonia solution. the samples were characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem) analyses after heat treatments. the sem results showed that, the size of the ito particles pr...

in this study, sio2 nanoparticles were successfully synthesized via sol-gel precipitation method and the effects of different parameters such as temperature, ethanol, ammonia and tetraethylorthosilicate (teos) contents based on water were investigated in a systematic way applying taguchi experimental design method. it was found that, among all the investigated parameters, ethanol as a co-solven...

The effect of the preparation method of Co/TiO2 catalysts on the performance in the liquid phase hydrogenation of cinnamaldehyde and crotonaldehyde has been studied. The Co/TiO2 catalysts were prepared by impregnation on titania (TiO2, P-25), sol-gel, and precipitation procedures. Different reduction-oxidation-reduction cycles were carried out in order to detect possible changes in the nature o...

The mechanisms responsible for spontaneous silver precipitation in silver-doped sol-gel materials are identified. The chemistry of the solvent phase is found to be the critical factor in controlling this phenomenon. The addition of HCl as catalyst leads to the formation of AgCl and subsequent formation of silver upon light exposure. Another factor leading to silver precipitation is the reducing...

The mechanisms responsible for spontaneous silver precipitation in silver-doped sol-gel materials are identified. The chemistry of the solvent phase is found to be the critical factor in controlling this phenomenon. The addition of HCl as catalyst leads to the formation of AgCl and subsequent formation of silver upon light exposure. Another factor leading to silver precipitation is the reducing...

Nanoparticles of lanthanum-strontium manganite were synthesized via different methods, namely, sol-gel method, precipitation from non-aqueous solution, and precipitation from reversal microemulsions. It was shown that the use of organic compounds and non-aqueous media allowed significantly decreasing of the crystallization temperature of nanoparticles, and the single-phased crystalline product ...

Controlling and engineering chemical structures are the most important scientific challenges in material science. Precipitation patterns from ions or nanoparticles are promising candidates for designing bulk structure for catalysis, energy production, storage, and electronics. There are only a few procedures and techniques to control precipitation (Liesegang) patterns in gel media (e.g., using ...

Se describen tres métodos para obtener hidroxiapatita (HA). La HA es una cerámica muy interesante por sus múltiples aplicaciones médicas. Los primeros dos métodos de precipitación parten de compuestos de calcio y fósforo, mientras que el tercer método es un proceso sol-gel que usa alcóxidos. Los productos fueron caracterizados y comparados entre sı́. Las diferencias observadas son importantes pa...