tio2 nanorods are synthesized by a thermal corrosion. in present work, synthesis of tio2 nanorods in anatase, rutile and ti8o15 phases, by using the sol-gel method and alkaline corrosion are reported. the morphologies and crystal structures of tio2 nanorods are characterized by use of field emission scanning electron microscopy, atomic force microscopy and x-ray diffractometer techniques. the o...

the composite powders of barium-magnesium ferrite were prepared using sol-gel auto-combustion and microwave methods. the crystal structure and the shape of nanocomposites have been compared. x-ray diffraction (xrd), scanning electron microscope (sem) and vibrating sample magnetometer (vsm) were used to investigate the structural, morphological and magnetic properties of nanopowder. the formatio...

in this investigation, fluor-hydroxyapatite (fha) film was deposited on a titanium substrate by sol-gel method. triethyl phosphite, ammonium fluoride and calcium nitrate in ethanol solutions were used respectively as p, f and ca precursors. typical apatite structures were obtained for all coatings after dipping and subsequent heat treatment at 550, 700 and 800 ºc, the coating layers were invest...

in the present investigation surface modification of silica nanoparticles by alumina was carried out by sol-gel process. fourier transform infrared (ftir) and x-ray fluorescence (xrf) confirmed the synthesis of silica and the surface modification as alumina is anchored to silica surface. field emission scanning electron microscopy (fesem) and transmission electron microscopy (tem) investigation...

transition-metal-substituted  (tms)  polyoxometalates  of  the  general  formula  [siw9m3o39], (where m = first row transition metal), has been synthesized and supported on anatase by sol–gel method under oil-bath condition. the tetrabutylammonium (tba) salts of the keggin-type polyoxotungstates  [siw9m3o39],  (m = vii, crii, mnii,  feii coii  and niii),  proved  to  be  green, reusable,  and  ...

structural properties and chemical composition change the photocatalytic activity in tio2-sio2 nanopowder composite. the sio2-tio2 nanostructure is synthesized based on sol–gel method. the nanoparticles are characterized by x-ray fluorescents (xrf), x- ray diffraction (xrd), tunneling electron microscopy (tem), field emission scanning electron microscopy (fe-sem), uv-vis. spectrophotometer and ...

in order to improve uv and visible lights photocatalytic activities of the pure anatase tio2, a novel and efficient n-doped tio2 photocatalyst was prepared by sol-gel method. n-doped titania is prepared using triethylamine (with difference molar ratios) as the nitrogen source. the crystalline structure, morphology, particle size, absorbance and band-gap and chemical structure of n-doped tio2 wa...

the silica supported platinum nanoparticles was synthesized by using the sol-gel method. the possibility of using diamminedinitro platinum (ii) as pt precursor and effect of metal precursor concentration on the final pt nanoparticle size was investigated. a stable silica sol was prepared via hydrolysis of tetraethyl orthosilicate (teos) as a metal alcoxide and condensation reaction. subsequentl...

highly crystalline bi3+-doped cadmium oxide (cdo) sub-micron structures were synthesized by calcination the obtained precursor from a sol-gel reaction. the reaction was carried out with cadmium nitrate (cd(no3)2.4h2o), bismuth nitrate (bi(no3)3.5h2o) and ethylene glycol (c2h6o2) reactants without any additives at 80°c for 2h. resulting gel was calcined at 900 °c with increasing temperature rate...

nano structured materials have wide range of applications due to their interesting size-dependent chemical and physical properties compared to particles of size in the range of micrometer. copper oxide nano materials are of interest on account of their potential uses in many technological fields. in this study  cuo nanoparticles were synthesized via simple sol gel method using basic cuso4 as we...