although several methods for the preparation of 4o propargyl indole derivatives have been published, this synthetic transformation is complicated by the tendency of 3o propargyl alcohols to form allenium intermediates in acidic media.  it is therefore a challenge to find an efficient method for the c-3 propargylation of indoles with 3° propargylic alcohols.  in this paper we wish to report on t...

PURPOSE Sodium bisulfate is known to affect the stability of octreotide. However, the critical concentration of sodium bisulfate is not known. Therefore, we assessed the critical concentration of sodium bisulfate needed to preserve the stability of octreotide using actual drugs containing sodium bisulfate. METHODS Although morphine and metoclopramide preparations are considered to be compatib...

Sodium bisulfate applied to horse bedding decreased ammonia levels, manure pH, and the number of flies when compared to a control period without sodium bisulfate. Behavior typical of ponies being bothered by flies (tail swishes, head tosses, and kicks or strikes) was also decreased when sodium bisulfate was used. Authors’ address: New Bolton Center, University of Pennsylvania, 382 West Street R...

Controlling Salmonella populations on commercial broiler grow out farms is a crucial step in reducing Salmonella contamination in processing plants. Broiler litter harbors many species of pathogenic bacteria including Salmonella. Sodium bisulfate has been shown to reduce concentration of bacteria in broiler litter. In experiments 1 and 2, sodium bisulfate was applied to broiler litter at rates ...

Different chemical formulations for the synthesis of highly intercalated graphite bisulfate have been tested. In particular, nitric acid, potassium nitrate, potassium dichromate, potassium permanganate, sodium periodate, sodium chlorate, and hydrogen peroxide have been used in this synthesis scheme as the auxiliary reagent (oxidizing agent). In order to evaluate the presence of delamination, an...

To measure nicotine personal exposure in our daily life, we have developed a determination method of personal exposure to nicotine. The method consisted of passive sampling of nicotine, simple solvent extraction and high performance liquid chromatography (HPLC) determination. The passive sampler was badge type and collection media was sodium bisulfate impregnated quartz fiber filter. The collec...

Two commercially available litter treatments, aluminum sulfate and sodium bisulfate, were tested to determine their effect on Campylobacter and Salmonella levels associated with commercial broilers during a 6-wk grow-out period. A total of 20 broiler houses at 10 different locations were studied; 5 aluminum sulfate-treated houses, 5 sodium bisulfate-treated houses, and 10 paired, untreated cont...

Two commercially available acidifying litter treatments, aluminum sulfate (alum) and sodium bisulfate, were tested to determine their effects on Campylobacter and Salmonella colonization frequencies and populations associated with broilers raised on treated pine litter. To produce contaminated litter, broiler chicks were inoculated with two bacterial cocktails (multistrain mixtures of campyloba...

Although several methods for the preparation of 4o propargyl indole derivatives have been published, this synthetic transformation is complicated by the tendency of 3o propargyl alcohols to form allenium intermediates in acidic media.  It is therefore a challenge to find an efficient method for the C-3 propargylation of indoles with 3° propargylic alcohols.  In this pa...