نتایج جستجو برای: Single-crystal X-ray diffractions
تعداد نتایج: 1592989 فیلتر نتایج به سال:
abstract: two new transition metal complexes, containing the acidic ligand 5-chlorosalicylic acid (h2l5), and 1,10-phenanthroline（phen） and 1,3-di(4-pyridyl)propane (bpp) as secondary ligands are reported. they are formulated as {[pb(hl5)2(phen)(h2o)]·h2o}n(1), [zn2(hl5)4(bpp)2]n(2). all the complexes are characterized by single-crystal x-ray diffractions. compoud 1 crystallizes in the triclini...
the structure of the nonaaquayttrium (iii) bromate, [y(h2o)9](bro3)3, at low temperature (100 k) has been studied by means of single-crystal x-ray diffraction. crystallography shows a hexagonal unit cell, space group p63/mmc (no. 194) with z = 2, a = b = 11.7104(11) å, c = 6.6259(5) å and v = 786.90(12) å3 at 100 k. the hydrated trivalent yttrium(iii) ion forms a tricapped trigonal prism, in wh...
In this paper, single-phase multiferroic ceramics of (1 x) BaTiO3 x BiFeO3 (BT x BFO) were synthesized by solid-solution method in the wide range of material composition (x1⁄4 0.025 – 1.0). The changes in crystal structure were confirmed via X-ray diffractions (XRD) and atomic pair distribution functions (PDFs). The room-temperature ME coupling was found to exhibit significant magnitude in the ...
the crystal structure of the title schiff base complex is obtained by single-crystal x-ray diffraction data.the solid state structure determination reveals that the coordination geometry around the copper(ii) center istetrahedrally distorted square-planar. the crystal packing shows one dimensional infinite chains which arisesfrom the intermolecular interaction and stabilize the crystal packing.
the structure of n,n'-bis(2-hydroxybenzylidene)-2,2-dimethyl-1,3-propanediamine, c19h22n2o2, has been studied at low temperature (120k) by means of single-crystal x-ray diffraction. solving the structure shows an orthorhombic unit cell, with p212121 space group, z = 4, a = 6.1046 (4) å, b = 15.8349 (11)å, c = 17.2898 (12) å and v = 1671.3 (2) å3. there are two relatively strong hydrogen bonds (...
in this paper, the structure of a new 16-membered macrocyclic schiff base compound n,n′-(3,3′-dimethoxy-2,2′-(propane-1,3-diyldioxy)dibenzylidene)propane-1,3-diamine, c22h26n2o4 (1), derived from 1,3-propanediamine and 3,3′-dimethoxy-2,2′-(propane-1,3-diyldioxy)dibenzaldehyde has been studied by single crystal x-ray diffraction, dft calculations at b3lyp/6-31g** and ft-ir spectroscopy. the titl...
The crystal structure of the title Schiff base complex is obtained by single-crystal X-ray diffraction data.The solid state structure determination reveals that the coordination geometry around the copper(II) center istetrahedrally distorted square-planar. The crystal packing shows one dimensional infinite chains which arisesfrom the intermolecular interaction and stabilize the crystal packing.
Nanoparticles of a new dinuclear silver(I) complex [Ag2(PPh3)2(μ-S-4nb-tsc)2(η1-S-4nb-tsc)2](NO3)2, where 4nb-tsc = 4-nitrobenzylidenethiosemicarbazone and PPh3 = triphenylphosphine, were prepared in an ultrasonic bath and characterized by FT-IR and SEM. The crystal structure of a suitable single crystal prepared by slow evaporation was determined by single crystal X-ray diffraction. The compou...
Abstract: Two new transition metal complexes, containing the acidic ligand 5-chlorosalicylic acid (H2L5), and 1,10-phenanthroline（phen） and 1,3-Di(4-pyridyl)propane (bpp) as secondary ligands are reported. They are formulated as {[Pb(HL5)2(phen)(H2O)]·H2O}n(1), [Zn2(HL5)4(bpp)2]n(2). All the complexes are characterized by single-crystal X-ray diffractions. Compoud 1 crystallizes in the triclini...
Advances in the fundamentals and applications of diffraction gratings have received much attention. However, conventional diffraction gratings often suffer from higher-order diffraction contamination. Here, we introduce a simple and compact single optical element, named inclined rectangular aperture gratings (IRAG), for quasi suppression of higher-order diffractions. We show, both in the visibl...
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