copper (ii) phthalocyanine and 2,9,16,23 tetrakis nitro copper (ii) phthalocyaninehas been synthesized respectively from phthalonitrile and 4-nitro phthalonitrile under solvent-free condition using two different catalystsovernanodimensionalzeolites. 4-nitro phthalonitrile synthesized from phthalimide in three steps. the newly prepared compounds have been characterized by ir, uv-vis, 1hnmr and m...

In the mol-ecule of the title compound, C(23)H(17)N(3)O(2), the methoxy-phenyl ring is oriented at dihedral angles of 13.34 (12) and 88.83 (12)° with respect to the methyl-phenyl and phthalonitrile rings, respectively; the dihedral angle between methyl-phenyl and phthalonitrile rings is 89.67 (10)°. In the crystal structure, weak inter-molecular C-H⋯N inter-actions link mol-ecules into chains. ...

Copper (II) phthalocyanine and 2,9,16,23 tetrakis nitro copper (II) phthalocyaninehas been synthesized respectively from phthalonitrile and 4-nitro phthalonitrile under solvent-free condition using two different catalystsovernanodimensionalzeolites. 4-Nitro phthalonitrile synthesized from phthalimide in three steps. The newly prepared compounds have been characterized by IR, UV-Vis, 1</sup...

Copper (II) phthalocyanine and 2,9,16,23 tetrakis nitro copper (II) phthalocyaninehas been synthesized respectively from phthalonitrile and 4-nitro phthalonitrile under solvent-free condition using two different catalystsovernanodimensionalzeolites. 4-Nitro phthalonitrile synthesized from phthalimide in three steps. The newly prepared compounds have been characterized by IR, UV-Vis, 1</sup...

Copper (II) phthalocyanine and 2, 9, 16, 23 tetrakis nitro copper (II) phthalocyanine has been synthesized respectively from phthalonitrile and 4-nitro phthalonitrile under solvent-free condition using two different catalysts over nanodimensional zeolites. 4-Nitro phthalonitrile synthesized from phthaimide in three steps. The newly prepared compounds have been characterized by IR, UV-Vis,1H N...

copper (ii) phthalocyanine and 2, 9, 16, 23 tetrakis nitro copper (ii) phthalocyanine has been synthesized respectively from phthalonitrile and 4-nitro phthalonitrile under solvent-free condition using two different catalysts over nanodimensional zeolites. 4-nitro phthalonitrile synthesized from phthaimide in three steps. the newly prepared compounds have been characterized by ir, uv-vis,1h nm...

Synthesis of metal-free and metallophthalocyanines bearing a-methylferrocenylmethoxy units was described. Precursor 3 required for the preparation of phthalocyanines 4–9, was synthsized by the nucleophilic aromatic substitution reaction between a-methylferrocenylmethanol and 4-nitrophthalonitrile in dry DMF. The metal-free phthalocyanine 4 was prepared from 4-(amethylferrocenylmethoxy)phthaloni...

In the title compound, C(21)H(12)ClN(3)O, the phenoxy ring makes dihedral angles of 51.42 (5) and 65.01 (6)°, respectively, with the chlorophenyl and phthalonitrile rings. In the crystal structure, the mol-ecules are inter-linked through weak C-H⋯N and C-H⋯π contacts, and π-π stacking inter-actions via crystallographic inversion centres form a three-dimensional network. The distance between the...

In the title compound, C(36)H(44)N(2)O(2), the dihedral angles between the phthalonitrile ring and the two di-tert-butyl-benzene rings are 68.134 (8) and 70.637 (11)°. The two nitrile groups are almost coplanar with the phthalonitrile ring except for one of the N atoms which deviates from the plane by 0.125 (4) Å. One of the tert-butyl groups is disordered over two orientations, with refined oc...

o-Phthalonitrile couples with chelating dioxime on nickel(II), with formation of a dinuclear nickel(II) macrocyclic complex--the first representative of a new class of imine-appended macrocycles.