The effect of ball-milling on physicochemical properties of maize starch was evaluated. Results found that the cold water solubility (CWS) of maize starch was positively correlated with the time of milling up to 3 h. There was no significant influence of using a ceramic pot versus a stainless steel pot on CWS. However, following 5 h of ball-milling CWS increased quite dramatically in the cerami...

AIM To illustrate the conceptual basis and the operative procedure of the Anatomic Endodontic Technology (AET) technique and to illustrate the specific instruments used in each phase. SUMMARY The basic characteristics of the AET technique are reported. The instruments and procedure are described in three phases: coronal access, coronal-middle preparation and apical preparation. In the first p...

The present work focuses on the mechanochemical preparation of industrially important β-cyclodextrin (CD) derivatives. Activated CDs have been reacted with nitrogen and sulfur nucleophiles using a planetary mill equipped with stainless steel, zirconia and glass milling tools of different sizes. It is shown that the milling frequency and the number as well as the size of the milling balls have a...

Ti Grade 2 was prepared by cryogenic attritor milling in liquid nitrogen and liquid argon. Two types of milling balls were used—stainless steel balls and heavy tungsten carbide balls. The effect of processing parameters on particle size and morphology, contamination of powder and its microhardness was investigated. Milling in liquid nitrogen was not feasible due to excessive contamination by ni...

Last years analytical or finite element models of milling become more efficient and focus on more physical aspects, nevertheless the milling process is still experimentally unknown on a wide range of use. This paper propose to analyse with accuracy milling operations by investigating the cutting forces values, shape of cutting forces curves obtained for different cutting speeds, and related phe...

Graphene materials have found applications in a wide range of devices over the past decade. In order to meet the demand for graphene materials, various synthesis methods are constantly being improved or invented. Ball-milling of graphite to obtain graphene materials is one of the many versatile methods to easily obtain bulk quantities. In this work, we show that the graphene materials produced ...

Mechanical alloying has recently attracted considerable attention as researchers strive to enhance nanocomposite properties and extend their utility. The process can be performed at room temperature and homogeneous nanocomposite powders can be produced. In this paper, we investigated the effect of different ball milling parameters and operating conditions (milling time, ball size, processing co...

Ultrafine MgH₂ nanocrystalline powders were prepared by reactive ball milling of elemental Mg powders after 200 h of high-energy ball milling under a hydrogen gas pressure of 50 bar. The as-prepared metal hydride powders were contaminated with 2.2 wt. % of FeCr-stainless steel that was introduced to the powders upon using stainless steel milling tools made of the same alloy. The as-synthesized ...

Obtaining finely ground, homogeneous plant and soil samples for chemical analysis without cross contamination is a major concern when using direct combustion procedures for determination of total nitrogen (N), total carbon (C), and isotope-ratio analysis. A rollermilling device, using square glass bottles instead of round grinding bottles, was evaluated. Rotation of the square bottles on the ro...

1569-190X/$ see front matter 2011 Elsevier B.V doi:10.1016/j.simpat.2011.10.009 ⇑ Corresponding author. Address: Laboratoire de M 42 27; fax: +33 (0) 4 91 16 44 81. E-mail address: [email protected] (A. Mau This paper describes investigations realised to perform simulations of shoulder milling operations on AISI 304L stainless steel using the commercial software LS-Dyna . A Lagrangian form...