in this study, isophthalic acid-zirconium(iv) nanocomposite has been prepared from zirconyl nitrate pentahydrate and potassium iodide, with isophthalic acid, (c8h6o4=benzene-1,3-dicarboxylic acid) as a ligand, via sonochemical method in ethylene glycol and methanol as solvents. the crystalline tetragonal zro2 has been produced by thermal decomposition of isophthalic acid-zirconium(iv) nanocompo...

sr5nb4o15 – nb2o5 nanocomposites were synthesized in 2 and 4 m koh aqueous solutions, via a non-stoichiometric 1:2 sr:nb molar ratio hydrothermal method at 160°c for 48 h (s1 and s2, respectively). sr(no3)2 and nb2o5 were used as raw materials. the synthesized nanomaterials were characterized by powder x-ray diffraction (pxrd) technique. it was found that sr5nb4o15 has been crystallized in hexa...

Recently, a cellulose-based composite material with a thin ZnO nanolayer-namely, ZnO nanocoated cellulose film (ZONCE)-was fabricated to increase its piezoelectric charge constant. However, the fabrication method has limitations to its application in mass production. In this paper, a hydrothermal synthesis method suitable for the mass production of ZONCE (HZONCE) is proposed. A simple hydrother...

sr6nb10o30–nb2o5 nanocomposite was synthesized in 2m naoh aqueous solution. a stoichiometric 1:1 sr:nb molar ratio hydrothermal method at 120°c was used to synthesize this nanocomposite. sr(no3)2 and nb2o5 were used as raw materials. the synthesized nanomaterials were characterized by powder x-ray diffraction (pxrd) technique. it was found that sr6nb10o30 was crystallized in tetragonal crystal ...

undoped and mn-doped zno nanoparticles were successfully prepared by the hydrothermal method with different annealing temperature conditions. structural, chemical and optical properties of the samples were studied by x-ray diffraction (xrd), field emission scanning electron microscopy (fesem), uv-vis spectrophotometry and fourier transform infrared (ft-ir) spectroscopy. the phase purity was con...

nano-sized batio3 powders with particular nb concentrations were prepared by rotary- hydrothermal (rh) method. hydrothermal method was used at 180 °c for 5 hours with new ti pressure and the teflon vessel was rotated at a speed of 160 rpm during the hydrothermal reaction. new hydrothermal method was used instead of previous solid state reaction for the system batio3±nb2o3 in high temperature to...

in this study, undoped zno and doped with fe and mn nanostructures were synthesized by hydrothermal method. the morphology of nanostructures was characterized by scanning electron microscope. the electrochemical response of the carbon paste electrode modified with nanoparticles of zno and also zno doped with fe and mn toward levodopa (l-dopa) was studied. studies of cyclic voltammetry using pro...

highly crystalline and pure lithium metasilicate (li2sio3) and lithium disilicate (li2si2o5) nanomaterials were synthesized by hydrothermal method and characterized by pxrd technique. the changes in the morphology and particle size of the synthesized nanomaterials with reaction time were investigated using sem technique. the uv-vis and photoluminescence spectra of the compounds were studied. th...