fecl3.6h2o was used as an efficient catalyst for the synthesis of highly functionalized piperidines via a one-pot five-component reaction of aromatic amines, aromatic aldehydes and β-keto esters in etoh at room temperature. the remarkable advantages offered by this method are good yields, simple procedure, short reaction times, no need to column chromatography and easy work-up. the structures o...

in this paper functionalized multiwall carbon nanotubes (fmwcnt) were modified using doxycycline, containing reactable nitrogen, which can attach chemically to functionalized mwcnt. the synthesized nano compounds were characterized by fourier transform infrared spectroscopy (ft-ir) and raman spectroscopy. these spectrums proved the existence of nitrogen atoms of amide functional groups. the mor...

This paper investigated the effect of the amine-functionalized carbon nanotubes (CNTs) on the thermomechanical properties of CNT/epoxy nanocomposites. Mechanical stirring and ultra-sonication were utilized to uniformly disperse CNTs into the epoxy matrix. Non-functionalized and amine-functionalized CNTs with different weight percentages (wt. %) were mixed into the epoxy resin. Using standard te...

the poly(ethyleneimine)-functionalized silica has been developed successfully as an effective adsorbent for the adsorption removal of cu(ii) ions from electroplating wastewater. the influences of ph, contact time and initial concentration of cu(ii) ions on the adsorption capacity and the effect of adsorbent dosage on the removal efficiency of cu(ii) ions from electroplating wastewater were inve...

in this work we synthesized nano hydroxyapatite (hap)  by sol-gel method, then we functionalized hydroxyapatite nanoparticle by use of  3-aminopropyl trimethoxysilane (aptms) , to improve the loading and control release of sulfasalazine drug bonded to aptms. the drug release patterns from sulfasalazine loaded hap nanoparticles at ph value 8 for 6h, sulfasalazine loaded functionalized hap nanopa...

in this work we synthesized of mesoporous silica nanoparticles and functionalized with 3-aminopropyltriethoxysilane to improve the loading and release of ibuprofen bonded to 3-aminopropyltriethoxysilane. sample were characterized by fourier transform infrared spectroscopy, scanning electron microscopy , x-ray diffraction, and ultraviolet-visible. the fourier transform infrared spectroscopy resu...

The poly(ethyleneimine)-functionalized silica has been developed successfully as an effective adsorbent for the adsorption removal of Cu(II) ions from electroplating wastewater. The influences of pH, contact time and initial concentration of Cu(II) ions on the adsorption capacity and the effect of adsorbent dosage on the removal efficiency of Cu(II) ions from electroplatin...

in this work, so3h-functionalizedphthalimide (sfp) as a so3h-containing solid acid is prepared by the reaction of phthalimide with chlorosulfonic acid, and characterized by ft-ir, 1h and 13c nmr, mass, tg, dtg, xrd and sem. then, it is utilized as a highly efficient, heterogeneous and green catalyst for the one-pot multi-component condensation of dimedone with arylaldehydes, β-ketoesters and am...

In this work we synthesized Nano hydroxyapatite (HAp)  by Sol-gel method, Then we functionalized hydroxyapatite nanoparticle by use of  3-Aminopropyl trimethoxysilane (APTMS) , to improve the loading and control release of sulfasalazine drug bonded to APTMS. The drug release patterns from Sulfasalazine loaded HAp nanoparticles at pH value 8 For 6h, Sulfasalazine loaded functionalized HAp nanopa...