In this study, the effect of operating parameters on dispersed phase holdup in liquid-liquid extraction process has been investigated. Three chemical systems (Toluene/Water, Butyl acetate/Water, and n-Butanol/Water) were utilized and holdup was considered in a wide range of interfacial tensions through a Scheibel extraction column. Various rotor speeds were examined on the certain velocities of...

Holdup was measured at various frequencies, amplitudes, continuous and dispersed phase flow rates for binary systems in a pulsed plate column capable of providing samples at various heights. The binary systems was so selected as to cover a wide spectrum of interfacial tensions. Dispersed phase holdup was found to increase with height in a logarithmic fashion at conditions away from the flooding...

In this work, the dispersed phase holdup in a Kühni extraction column is predicted using intelligent methods and a new empirical correlation. Intelligent techniques, including multilayer perceptron and radial basis functions network are used in the prediction of the dispersed phase holdup. To design the network structure and train and test the networks, 174 sets of experimental data are used. T...

an experimental study of the phase inversion behavior of liquid-liquid dispersion has been conducted in a spray extraction column for systems of toluene / water, n-hexane/water, ccl4/water, toluene /water + glycerol (25 % wt), toluene + ccl4 (25 % wt) / water and toluene / acetic acid (5 % wt)/water. the effects of physical properties, mass transfer and column geometry on phase inversion have b...

An experimental study of the phase inversion behavior of liquid-liquid dispersion has been conducted in a spray extraction column for systems of toluene / water, n-hexane/water, CCl4/water, toluene /water + glycerol (25 % wt), toluene + CCl4 (25 % wt) / water and toluene / acetic acid (5 % wt)/water. The effects of physical properties, mass transfer and column geometry...

In this work, feasibility of flow pattern and oil holdup prediction for vertical upward oil–water two–phase flow using pressure fluctuation signals was experimentally investigated. Water and diesel fuel were selected as immiscible liquids. Oil holdup was measured by Quick Closing Valve (QCV) technique, and five flow patterns were identified using high speed photography through a transparent tes...

Steady-state and transient experiments of water–gas, oil–water and oil–water–gas multiphase flows were conducted on a transparent 11 m long, 15 cm diameter, inclinable pipe using kerosene, tap water and nitrogen. The pipe inclination was varied from 0 (vertical) to 92 and the flow rates of each phase were varied over wide ranges. Fast-acting valves enabled the trapping of the fluid flowing in t...

In this work, the feasibility of flow pattern and oil hold up the prediction for vertical upward oil–water two–phase flow using pressure fluctuation signals was experimentally investigated. Water and diesel fuel were selected as immiscible liquids. Oil hold up was measured by Quick Closing Valve (QCV) technique, and five flow patterns were identified using high-speed photo...

This work provides a review of hydrodynamic characteristics and mass transfer in the K?hni extraction columns. The experiments, as reported literature, were performed presence absence transfer. results showed that Sauter mean drop diameter was strongly affected by rotor speed interfacial tension, whereas effects dispersed continuous velocities negligible. Empirical correlations for diameter, ta...