in this study, the effect of recrystallization of naproxen in the presence of hydroxypropyl cellulose (hpc) on the release rate of drug was investigated. crystals were generated by the anti-solvent approach using the hpc solution in water as the anti-solvent. the samples were subjected to various physicochemical evaluations such as crystal size, scanning electron microscopy, fourier transform i...

It has been shown experimentally by many researchers that cooling rate and crystallization temperature affect the rate of crystal formation. In this study, crystallization kinetics of coconut oil was measured by monitoring the solid fraction of the oil using pulsed Nuclear Magnetic Resonance (pNMR). Four levels of cooling rate and crytallization temperature were studied. Parameters of crystalli...

based on driving force for crystallization of one-component gas hydrate, in this report an expression for the supersaturation for crystallization of multicomponent gas hydrate is derived. expressions for the supersaturation are obtained in isothermal and isobaric regimes. the results obtained are applied to the crystallization of hydrates of mixtures of methane plus ethane and can apply to othe...

Crystallization chaperones have been used to facilitate the crystallization of challenging proteins. Even though the maltose-binding protein (MBP) is one of the most commonly used crystallization chaperones, the design of optimal expression constructs for crystallization of MBP fusion proteins remains a challenge. To increase the success rate of MBP-facilitated crystallization, a series of expr...

transparent glasses in a system of li2o-mgo-sio2-al2o3-fchemical constituents were prepared by melt quenching method. in the fabrication of nanocrystal glass-ceramics, controlled nucleation and subsequent crystal growth were necessary to avoid loss of transparency. it was therefore important to understand thermal properties and crystallization kinetics of the glass ceramics. the crystallization...

We have observed 2D protein crystallization under conditions where in the absence of flow, crystallization fails to occur. Even under conditions where crystallization does occur in quiescent systems, we have found that flow can accelerate the crystallization process. By interrogating the flow responsible for this enhanced crystallization, we have correlated the enhancement with large shear in t...

Isothermal melt crystallization kinetics of PVDF was investigated by differential scanning calorimetry. Thin PVDF film has been fabricated by the solvent casting technique using dimethylformamide (DMF). Then, the samples were melted and subsequently crystallized in the range of the crystallization temperature (Tc) between 138 and 145 °C. The crystallization kinetics was derived from Avrami equa...

non-isothermal crystallization kinetics of polypropylene (pp) and pp containing 0.5 wt% singlewalled carbon nanotubes (pp/swnt) were studied at various cooling rates using differential scanning calorimetry technique. the non-isothermal melt crystallization data were analyzed according to ozawa and cazé-chuah models. although ozawa model was successful in describing the nonisothermal crystalliza...

The structure evolutions of Al83Ni10Ce5Si2, Al83Ni10Ce7, Al85Ni10Ce5, Al87Ni7Nd6 and Al87Ni5Co2Nd6 metallic glasses have been studied in detail. The studies establish a relation between the amount of medium range order (MRO) and crystallization mode. An increased amount of MRO suppresses the precipitation of primary fcc-Al and transforms the crystallization mode from a primary crystallization (...

Atomistic understanding of crystallization in solids is incomplete due to the lack of appropriate materials and direct experimental tools. Metallic glasses possess simple metallic bonds and slow crystallization kinetics, making them suitable to study crystallization. Here, we investigate crystallization of metallic glass-forming liquids by in-situ heating metallic glass nanorods inside a transm...