the kinetics of molybdenite oxidation was studied by non-isothermal tga-dta with heating rate 5 ºc.min-1.the model-fitting kinetic approach applied to tga data .the coats-redfern method used for model fitting. the popular model-fitting gives excellent fit for non-isothermal data in chemically controlled regime. the apparent activation energy was determined to be about 34.2 kcalmol-1 with pre-ex...

824 | CrystEngComm, 2015, 17, 824–829 This journal is © The R a BAM Federal Institute for Materials Research and Testing, Richard-WillstaetterStr. 11, 12489 Berlin, Germany. E-mail: [email protected] Department of Chemistry, Humboldt-Universität zu Berlin, Brook-Taylor-Str. 2, 12489 Berlin, Germany † Electronic supplementary information (ESI) available: DTA-TGA measurements of the reac...

The thermogravimetric analysis (TGA) and the differential thermal analysis (DTA) were applied to investigations of aging processes in some electroinsulating polymeric materials (glass reinforced epoxy resin, NBR ( two sorts), styrenated unsatured polyester resin, hydrogenated NBR (T80), polychloroprene rubber , EPR) and to the measurement of aging reaction rates. It is shown that thermal analys...

Article history: Received on: 29/05/2014 Revised on: 12/06/2014 Accepted on: 30/06/2014 Available online: 28/07/2014 In this study effect of gamma irradiation sterilization and storage conditions on thermal properties of phase sensitive granisetron in situ forming implant (ISFI) was investigated. ISFI was prepared by mixing Poly (DLlactide-co-glycolide) (PLGA) with dimethylsulfoxide (DMSO) : pr...

The thermal characteristics of seven crystals with [Ni(NCS),(vpy),] (vpy = 4-vinylpyridine) as host were analysed by thermal gravimetric analysis (TGA) and differential thermal analysis (DTA). N o preferential guest loss for the clathrates with pairs of guests was observed. The enthalpy of the 'guest release reaction' for each clathrate was obtained from the DTA experiments. Solubility studies ...

b1-xlaxfeo3 (x = 0.0, 0.025) crystallites were prepared by chemical solution route. xrd analysis confirmed the phase formation of the materials. thermal characterization was done by dsc-tga to confirm crystallization and thermal behavior for phase development. morphological studies by fesem showed the agglomerated nature of the ferrite and edx analysis confirmed the degree of doping. ftir studi...