aprotic diazotization of anthranilic acid with isoamylnitrite or amylnitrite gave benzenediazonium-2- carboxylate. subsequent thermal decomposition of this diazonium salt (in situ) in 1,2-dichloroethane as a solvent at 85oc and in the presence of 2,5-diethyl-3,4-diphenylcyclopentadienonaes a trapping agent gave 1,4-diethyl-2, 3-diphenylnaphthalene in high yield, after loss of carbon monoxide. a...

Composite solid propellants were prepared with and without nano-alloys (Ti-Co, Ti-Ni, Ti-Zn), where nano-alloys used as catalyst. These nano-alloys are prepared by hydrazine reduction method. Catalytic properties of these nanomaterials were measured on Ammonium perchorate/hydroxyterminatedpolybutadiene propellant by thermogravimetery analysis and differential thermal analysis. Both experimental...

This paper presents in a comprehensive way the thermal behavior of natural and hot-.washed sisal fibers, based on the fundamental components of lignocellulosic materials: cellulose, xylan and lignin. The research highlights the influence exerted on the thermal stability of sisal fibers by other constituents such as non-cellulosic polysaccharides (NCP) and mineral matter. Thermal changes were in...

in this paper, the mer-co(nh3)3(no2)3 complex was used as a new precursor for synthesizing spinel-type cobalt oxide nanoparticles (co3o4nps).thermal decomposition of the complex at low temperature (175 °c) resulted in the co3o4nps without using expensive and toxic solvents or complicated equipment. xrd, ft-ir, sem, edx, and tem were employed to characterize the product, and its optical and magn...

in this paper, the nonlinear differential equation for the convection of the temperature distribution of a straight fin  with the thermal conductivity depends on the temperature is solved using adomian decomposition method and padé approximation(padm) for boundary problems. actual results are then compared with results obtained previously  using digital solution by runge–kuttamethod and a diffe...

The thermal reaction of SF 6 with tungsten powder was investigated by thermogravimetry (TG) and differential scanning calorimetry (DSC), combined the characterization solid decomposition products SEM, EDS, XPS Raman. Based on above experiments, a two-stage process proposed: first stage is surface vulcanization W+SF →S 2 , mainly taken place at 600 °C, activation energy valued 152.8 kJ·mol -1 ac...

Composite solid propellants were prepared with and without nano-alloys (Ti-Co, Ti-Ni, Ti-Zn), where nano-alloys used as catalyst. These nano-alloys are prepared by hydrazine reduction method. Catalytic properties of these nanomaterials were measured on Ammonium perchorate/hydroxyterminatedpolybutadiene propellant by thermogravimetery analysis and differential thermal analysis. Both experimental...