The work was aimed at the investigation of kinetics Spark Plasma Sintering (SPS) α-Al2O3 particles with amorphous surface layers and effect on grain growth mechanical properties alumina. objects investigations comprised:(i) submicron powder, (ii) powder particles' surfaces, (iii) fine-grained powder. powders (i) were used to analyze sintering kinetics. Powders initial particle sizes shrinkage t...

Transparent yttrium aluminum garnet (YAG) ceramics doped with cerium ions (Ce3+) were successfully synthesized using the spark plasma sintering (SPS) process at a temperature of 1600 °C, isothermal exposure 10 minutes, pressure 100 MPa and heating rate °C/min from mechanical mixture powders yttrium, aluminum, oxides. Transmittance in visible range for 1 mm thick samples is above 40 %; near infr...

In order to improve the mechanical properties of B4C ceramics, B4C@TiB2 composite powders with core-shell structure are prepared by molten salt method using and Ti as raw materials. And ceramics were from spark plasma sintering (SPS). The results show that exhibit intact structure. improves mass transfer during sintering. When molar ratio B4C/Ti is 2/1, relative density, Vickers hardness, fract...

Over the past two decades several nano-structuring methods have helped improve the figure of merit (ZT) in the state-of-the art bulk thermoelectric materials. While these methods could enhance the thermoelectric performance of p-type Bi2Te3, it was frustrating to researchers that they proved ineffective for n-type Bi2Te3 due to the inevitable deterioration of its thermoelectric properties in th...

P-type SnS compound and SnS1-xSex solid solutions were prepared by mechanical alloying followed by spark plasma sintering (SPS) and their thermoelectric properties were then studied in different compositions (x = 0.0, 0.2, 0.5, 0.8) along the directions parallel (//) and perpendicular (⊥) to the SPS-pressurizing direction in the temperature range 323-823 Κ. SnS compound and SnS1-xSex solid solu...

XNiSn (X = Ti, Zr and Hf) half-Heusler alloys have promising thermoelectric properties and are attracting enormous interest for use in waste heat recovery. In particular, multiphase behaviour has been linked to reduced lattice thermal conductivities, which enables improved energy conversion efficiencies. This manuscript describes the impact of spark plasma sintering (SPS) on the phase distribut...

The data presented in this article are related to the research article entitled "Cyclic Shear behavior of conventional and harmonic structure-designed Ti-25Nb-25Zr β-titanium alloy: Back-stress hardening and twinning inhibition" (Dirras et al., 2017) [1]. The datasheet describes the methods used to fabricate two β-titanium alloys having conventional microstructure and so-called harmonic structu...

Cu3SbSe3-based composites have been prepared by self-propagating high-temperature synthesis (SHS) combined with spark plasma sintering (SPS) technology. Phase composition and microstructure analysis indicate that the obtained samples are mainly composed of Cu3SbSe3 phase and CuSbSe2/Cu2–xSe secondary phases. Our results show that the existence of Cu2–xSe phase can clearly enhance the electrical...

Advisor: Bai Cui Molybdenum aluminum boride (MoAlB) is a ternary transition metal boride which has promising aeronautic and nuclear applications. It inheres excellent properties of the binary transitional metal borides (e.g., MoB, ZrB2) such as high melting temperature, high hardness, and thermal conductivity. Besides, MoAlB is superior to MoB because: (1) the Al element provides an oxidation r...

High-density fine-grained Ni0.5Zn0.5Fe2O4 ferrite ceramics were synthesized by spark plasma sintering (SPS) in conjunction with high energy ball milling. The precursor powders were milled for 20 h, 40 h, and 60 h, respectively, and the milled powders were all sintered for 5 min at 900 ̊C. All the samples exhibit a single spinel phase. With increasing of the ball milling time, the relative densit...