In the present work, we have planned a new magnetically recoverable nanocatalyst. The obtained nanocatalyst designated as Fe3O4@SiO2@DOPisatin-Ni (II) was characterized by FTIR, XRD, SEM, EDAX, VSM, AAS and TGA techniques. It was found that Fe3O4@SiO2@DOPisatin-Ni (II) successfully catalyses the synthesis of 2,3-dihydroquinazolin-4(1H)-ones, polyhydroquinoline and 5-substituted 1H-tetrazoles in...

sulfonic acid functionalized sba-15 as a nanoporous acid catalyst was used in the synthesis of 2-aryl benzoxazoles 4 by the condensation of 2-aminophenol 1 and benzoyl chlorides 2 under microwave irradiation in solvent free reaction conditions. the advantages of this methodology are good product yields (60-98%), being environmentally benign, short reaction times and easy work up.

poly(4-vinylpyridine)-supported copper iodide nanoparticles is reported as a new, green and recyclable catalyst for the synthesis of aryl-14h-dibenzo [a-o] xanthenes under solvent-free conditions. this catalyst can be recovered by simple filtration and recycled up to 8 consecutive runs without any loss of their efficiency.

A irradiação de chalconas com microondas na ausência de solvente se mostrou um procedimento de “química verde” para a preparação, em bons rendimentos, de flavanonas. Diferentes catalisadores heterogêneos e catalisadores convencionais foram testados usando-se um forno de microondas doméstico. A irradiação de chalconas com 30% de ácido trifluoroacético, na presença de gel de sílica, levou a forma...

a phosgene-free synthesis of symmetrical n,n'-disubstituted urea by the reaction of aromatic and aliphatic primary amines and urea promoted by  microwave irradiation in the presence of a suitable energy-transfer solvent such as n-n-dimethylacetamide is described.

ammonium monovanadate (nh4vo3) has been devoted as an efficient, commercially available, eco-friendly and reusable catalyst for the synthesis of bis(indolyl)methanes (bims), oxindole derivatives and also michael adducts of indoles at 50 °c under solvent-free conditions. the reusability of this solid acid catalyst in addition with its selectivity has also been examined.

a simple and efficient procedure has been developed for the synthesis of 2,3-dihydroquinazolin-4(1h)-ones derivatives under solvent-free conditions. this method uses the condensation of isatoic anhydride, aldehydes, and amines in the presence of a catalytic amount sulfonated porous carbon (spc). one of the important advantages of the new method is that the spc could be recycled and reused.

An efficient synthesis route to 1,4-dihydropyrimidine derivatives from reaction of divergent aldehydes with ethylacetoacetate and urea under solvent-free conditions by ZnO nanoparticles as a relative in expansive, eco-friendly, easy available, non-volatile, non-explosion, thermally robust, recyclable and easy to handle catalyst at 90°C with excellent yields is described. Unenhanced reaction tim...

An efficient synthesis route to 1,4-dihydropyrimidine derivatives from reaction of divergent aldehydes with ethylacetoacetate and urea under solvent-free conditions by ZnO nanoparticles as a relative in expansive, eco-friendly, easy available, non-volatile, non-explosion, thermally robust, recyclable and easy to handle catalyst at 90°C with excellent yields is described. Unenhanced reaction tim...

Mesoporous photocatalysts of CeO2/SBA-15 are prepared by two methods of direct synthesis as solvent-usage and solvent-free methods. In solvent-usage method, CeO2/SBA-15 is synthesized in acidic media. While, in solvent-free method, CeO2/SBA-15, has been prepared through the novel path of directly grind cerium salt into the as-prepared samples of SBA-15 occluded ...