نتایج جستجو برای: quinolines multicomponent reaction molecular iodine

تعداد نتایج: 1036260  

Journal: :iranian journal of pharmaceutical research 0
ghodsi mohammadi sakineh faramarzi alzahra university shima asadi alzahra university massoud amanlou tehran university

sulfonic acid functionalized sba-15 (sba-pr-so3h) with pore size 6 nm as an efficient heterogeneous nanoporous solid acid catalyst exhibited good catalytic activity in the biginelli-like reaction in the synthesis of spiroheterobicyclic rings with good yield and good recyclability. spiro-pyrimidinethiones/spiro-pyrimidinones-barbituric acid derivatives were synthesized in a simple and efficient ...

2018
Kasra Amini Evgeny Savelyev Felix Brauße Nora Berrah Cédric Bomme Mark Brouard Michael Burt Lauge Christensen Stefan Düsterer Benjamin Erk Hauke Höppner Thomas Kierspel Faruk Krecinic Alexandra Lauer Jason W. L. Lee Maria Müller Erland Müller Terence Mullins Harald Redlin Nora Schirmel Jan Thøgersen Simone Techert Sven Toleikis Rolf Treusch Sebastian Trippel Anatoli Ulmer Claire Vallance Joss Wiese Per Johnsson Jochen Küpper Artem Rudenko Arnaud Rouzée Henrik Stapelfeldt Daniel Rolles Rebecca Boll

We explore time-resolved Coulomb explosion induced by intense, extreme ultraviolet (XUV) femtosecond pulses from a free-electron laser as a method to image photo-induced molecular dynamics in two molecules, iodomethane and 2,6-difluoroiodobenzene. At an excitation wavelength of 267 nm, the dominant reaction pathway in both molecules is neutral dissociation via cleavage of the carbon-iodine bond...

Journal: :Organic & biomolecular chemistry 2013
Marko Weimar Matthew J Fuchter

The challenging coupling of 10-halobenzo[h]quinolines with ortho-substituted aryl boronic acids has been achieved using Pd(OAc)(2)/P(O)Ph(3) as the catalytic system. High yields were obtained for diversely functionalised substrates under mild reaction conditions.

Journal: :Organic Letters 2021

An operationally simple, high yielding three-step cascade process is described for the direct conversion of indole-tethered ynones into functionalized quinolines. A single “multitasking” thiol reagent used to promote a dearomatizing spirocyclization, nucleophilic substitution, and one-atom ring expansion reaction under remarkably mild conditions. In addition, novel route thio-oxindoles describe...

Journal: :Organic letters 2014
Qin Yang Tongyu Xu Zhengkun Yu

FeCl3- and FeBr3-mediated tandem carboarylation/cyclization of propargylanilines with diethyl benzaldehyde acetals furnished the tetracyclic core of indeno[2,1-c]quinolines. 5-Tosyl-6,7-dihydro-5H-indeno[2,1-c]quinoline and 7H-indeno[2,1-c]quinoline derivatives were obtained in good to excellent yields, respectively, by tuning the FeX3 loadings and/or reaction temperatures.

Journal: :Chemical communications 2012
Zhenjun Mao Haijun Qu Yanyan Zhao Xufeng Lin

1,1-Cyclopropane aminoketones were efficiently synthesized in high yields by the tandem reaction of α-amino aryl ketones with vinyl sulfonium salts using DBU as the base in CH(2)Cl(2). This methodology was utilized to synthesize 2-benzoyl quinolines.

Mohammad Yari Omid Moradi S. Sedaghat

In this research we used Heavy Propylene Tetramer (HPT) and A1C13 —BF3 (Lewis acids) ascatalyst and ethanol, n-propanol and n-butanol as co-catalyst. Using Lewis acids as catalyst, theHPTs form molecules with higher molecular weight. Since the raw materials of the reaction are byproducts of other reactions, are not pure and contain various compounds with different M.W andalso different chemical...

Journal: :iranian journal of catalysis 2014
hossein eshghi zaiddodine pashandi gholam hossein rounaghi afsaneh alipour azadeh shafaie

the regioselective ring opening of styrene oxide using elemental iodine and bromine in the presence of disulfides as new catalysts was studied. the conductivity titration and uv spectroscopy were used to study the interaction of iodine with these catalysts. the results indicate that disulfide 11 is efficient in polyiodide formation, and can catalyze this reaction in excellent yield and high reg...

Afsaneh Alipour Azadeh Shafaie Gholam Hossein Rounaghi Hossein Eshghi Zaiddodine Pashandi

The regioselective ring opening of styrene oxide using elemental iodine and bromine in the presence of disulfides as new catalysts was studied. The conductivity titration and UV spectroscopy were used to study the interaction of iodine with these catalysts. The results indicate that disulfide 11 is efficient in polyiodide formation, and can catalyze this reaction in excellent yield and high reg...

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