The structure of nano-crystalline Fe2O3 particles, synthesized using the microwave plasma technique, has been analysed using synchrotron based X-ray absorption spectroscopy and X-ray powder diffraction, as well as transmission electron microscopy. Furthermore, magnetic properties, the crystal structure, and the microstructures are compared and the potential model character of the samples for st...

Porous yttria-stabilised zirconia ceramics have been gaining popularity throughout the years in various fields, such as energy, environment, medicine, etc. Although yttria-stabilised zirconia is a well-studied material, voided yttria-stabilised zirconia powder particles have not been demonstrated yet, and might play an important role in future technology developments. A sol-gel synthesis accomp...

BACKGROUND Many researchers have tried to enhance materials functions in different aspects of science using nano-modification method, and in many cases the results have been encouraging. To evaluate the histopathological responses of the micro-/nano-size cement-type biomaterials derived from calcium silicate-based composition with addition of nano tricalcium aluminate (3CaO.Al2O3) on bone heali...

This paper systematically studied the modification of cement-based materials by nano-SiO₂ particles with an average diameter of about 20 nm. In order to obtain the effect of nano-SiO₂ particles on the mechanical properties, hydration, and pore structure of cement-based materials, adding 1%, 3%, and 5% content of nano-SiO₂ in cement paste, respectively. The results showed that the reaction of na...

In the present work, the activity of sono-catalytic synthetic nano-sized ZnO powder was studied via degradation of Direct Blue71 (DB71), an organic compound, as a case study. Nano-sized ZnO powder was synthesized without high-temperature activation then introduced to act as the sono-catalyst. Different characterization analyses were applied to demonstrate and confirm the structure of synthetic ...

nano-srtio3 and tio2 powders were synthesized using sol-gel method. the srtio3 and tio2 powders were characterized using xrd, sem, and spectrophotometry. xrd analysis indicated that the tio2 powder was uniform anatase crystals of 9.9 nm and the srtio3 powders was cubic nano-crystal of 16.2nm. photocatalytic experiments revealed that methyl orange in water can be decomposed on the two powders un...

design and synthesis of high-performance hydrogenstorage materials. Although the weakest X-ray scattering amplitude of hydrogen made it difficult to determine their structure, we have succeeded in the first direct observation of elusive H2 molecules adsorbed in the nano-channels of a metal-organic porous material by the in situ synchrotron powder diffraction experiment of gas adsorption and by ...

a novel complex of cadmium (ii) [cdl0.5(no3)(h2o)](1), l= n,n-bis (o-hydroxyacetophenone) ethylene diamine, have been synthesized as single crystal and nano size. compound 1 in nano size was obtained under sonochemical irradiation and has been characterized by ir, 1hnmr spectroscopy, x-ray powder diffraction (xrd) and scanning electron microscopy (sem). the gray single crystal of compound 1 has...

Two nano-sized mixed-ligand Cd (II) coordination polymers; [Cd (4,4' -bpy) (C4H4O4)].1/4 H2O (1) and[Cd(bpy)1.5 (NO3)2].3H2O (2) (bpy=bipiridine) were synthesized by a sonochemical method and characterized by elemental analyses, thermal gravimetric analysis (TGA), differential thermal analysis (DTA), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR). The cry...