Intermetallide phase formation was studied in a powdered Fe–Al system under layer by layer laser cladding with the aim of fabricating the gradient of properties by means of changing the Fe–Al concentration ratio in the powder mixture from layer to layer. The relationships between the laser cladding parameters and the intermetallic phase structures in the consecutively cladded layers were determ...

The manganese ferrite spinel was synthesized by co-precipitation. The nano sized manganese ferrite characterized by X-ray diffraction (XRD), Scanning electron micrograph (SEM), tunneling electron micrograph (TEM) and Energy dispersive X-ray (EDX) techniques. The adsorption ability of malachite green (MG) from the aqueous solution by manganese ferrite was investigated. It was found that pH value...

Titanium carbide-graphite (TiC/C) composite was successfully synthesized from Ti and C starting elemental powders using self-propagating high-temperature synthesis technique in an ultra-high plasma inert medium in a single stage. The TiC was exposed to a high-temperature inert medium to allow recrystallization. The product was then characterized using field emission scanning electron microscopy...

Samarium-doped ZnO hierarchical micro/nanospheres (Sm/ZnO) were synthesized via a facile and surfactant-free chemical solution route. The obtained products were characterized by field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), energy dispersive X-ray (EDX), UV–visible diffuse reflectance spectroscopy (UV-vis DRS) and photolumi...

in this study, tio2 and zno nanofilms were prepared by sol-gel spin-coating method. nanofilms were characterized by x-ray diffraction (xrd), energy dispersive analysis of      x-ray (edx), scanning electron microscopy (sem) and field emission scanning electron microscopy (fe-esm). structural and morphological properties of nanofilms were investigated. the average crystalline size of tio2 and zn...

in this research, the thin films of n-s doped titanium dioxide (tio2) were successfully prepared by simple sol-gel method in the presence of tetrabutylorthotitanate as a starting reagent. furthermore, titanium dioxide (tio2) was functionalized with thiourea. furthermore, n-s doped titanium dioxides (nsto) were fixed on glass balls by glass balls fixed-bed reactor system. besides, the effect of ...

CuInS2 nanostructures were  synthesized  via  a  simple  surfactant-free solvothermal  route.  In  this  synthesis,  thiosemicarbazide  and thioglycolic acid were used as sulfur sources. The effects of different parameters such as type of precursor and time on the morphology and particle  size  of  the  samples  have  been  investigated.  The nanostructures  were  characterized  by  means ...

Phthalimide was reacted with chlorosulfonic acid to give sulfonic acid-functionalized phthalimide (SFP), which characterized by 1H NMR, 13C NMR, FT-IR, XRD (X-ray diffraction), SEM (scanning electron microscopy), EDX (energy-dispersive X-ray), mass, TG (thermogravimetry) and DTG (derivative thermal gravimetry) spectra. Afterward, its catalytic activity was examined for the condensation of aryla...

Abstract-In-situ chemical polymerization was used to synthesize PPy/ TiO2 nanocomposite. The nanocomposite was characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, Scanning electron microscopy (SEM) and Energy dispersive X-ray spectroscopy (EDX) to ensure the crystallite size, functional groups and morphology of the polymer nanocomposite. The band gap of th...

CuIn2n+1S3n+2 crystals were synthesized by horizontal Bridgman method using high purity copper, indium, sulfur elements. The phases and crystallographic structure of the CuIn2n+1S3n+2 crystals were analyzed by X-ray diffraction (XRD) and the composition of the material powders was determined using the energy dispersive X-ray analysis (EDX). Measurement data revealed that CuIn2n+1S3n+2 materials...