One of the principal problems with nano-crystalline materials is producing them in quantities and sizes large enough for valid mechanical property evaluation. The purpose of this study was to explore an innovative method for producing nano-crystalline γ-TiAl bulk materials using high energy ball milling and brief secondary processes. Nano-crystalline powder feedstock was produced using a Fritsc...

the perovskite-type oxides strontium-substituted lanthanum nickelate (lsno) were prepared by a coprecipitation method in the present of octanoic acid as surfactant. the phase composition, morphology,lattice parameters and size of nanoparticles in these materials were characterized through fourier transform infrared spectroscopy (ft-ir), x-ray diffraction (xrd), scanning electron microscopy (sem...

Natural Akermanite (NAM) has been successfully prepared by a modified sol-gel method. Optimization in calcination temperature and mechanical ball milling resulted in a pure and nano-sized powder which characterized by means of scanning electron microscopy (SEM), X-ray diffraction (XRD), transmission electron microscopy (TEM) and Fourier transform infrared Spectroscopy (FT–IR). Calcium nitrate, ...

High-density fine-grained Ni0.5Zn0.5Fe2O4 ferrite ceramics were synthesized by spark plasma sintering (SPS) in conjunction with high energy ball milling. The precursor powders were milled for 20 h, 40 h, and 60 h, respectively, and the milled powders were all sintered for 5 min at 900 ̊C. All the samples exhibit a single spinel phase. With increasing of the ball milling time, the relative densit...

in this research nanoparticles of nickel (ii) chloride were synthesized and characterized using fourier transform infrared (ft-ir) spectra. nanoparticles of nickel (ii) chloride were prepared by using of ball mill device. a ball mill is one kind of grinding machine, and it is a device in which media balls and solid materials (the materials to be ground) are placed in a container. in the researc...

in this research, the high-energy planetary mill was employed to produce nanocrystalline ti-50al(γ)(at%) powders. initial powders were mechanically alloyed in 99.9999% and 90% purities of argon and also air atmosphere with alloying times up to 50h. the effect of impurity of argon atmosphere on the microstructure and the rate of phase transformation of ti-50al were investigated during mechanical...

We report on the synthesis, morphology, chemically and structurally of TiO2-NiO-SiO2 nanostructure. The TiO2-NiO-SiO2 nanostructure was synthesized by a method based on the sol-gel method, by the simultaneous gelation of all cations. The coatings were deposited on dried soda-lime glass slides by spin coating. Composite powders and coating on glass hav...