The mesoporous metal-organic frameworks are a family of materials that have pore sizes ranging from 2 to 50 nm, which have shown promising applications in catalysis, adsorption, chemical sensing and so on. The preparation of mesoporous metal-organic frameworks usually needs the supramolecular or cooperative template strategy. Here we report the template-free assembly of mesoporous metal-organic...

Supercritical fluid extraction analyses are often compromised by trace impurities present in the solvent carbon dioxide. These impurities, commonly used as lubricants in the specialty gas industry, can produce significant background levels, increasing limits of detection and quantification. This problem is especially severe when electron capture detection (ECD) is used for trace concentrations ...

Swelling/extraction tests are single-contact phase-behavior experiments to measure the solubility of CO2 dissolved in crude oil and the amount of hydrocarbon that CO2 can extract or vaporize from crude oil. The tests are commonly conducted in a visual PVT cell with a large sample size (40-100cc). In this paper, an easy operated apparatus capable of determining phase behavior with a significantl...

Cat's whiskers (Orthosiphon stamineus) leaves extracts were prepared using supercritical CO2 (SC-CO2) with full factorial design to determine the optimum extraction parameters. Nine extracts were obtained by varying pressure, temperature, and time. The extracts were analysed using FTIR, UV-Vis, and GC-MS. Cytotoxicity of the extracts was evaluated on human (colorectal, breast, and prostate) can...

a pressurized fluid extraction (pfe) method for the extraction of pistachio oil was developed using a modified supercritical fluid extractor. the supercritical fluid extraction apparatus was modified to be able to pump liquid solvent and co2 into the extraction vessel alternatively. the experimental results showed that the extraction yield was independent of the extraction pressure. it was also...

The subcritical fluid extraction of lovastatin from tablet powder mixtures prepared in this laboratory and MEVACOR tablets is successfully demonstrated. Methanol modifier percentage, additive type (acidic, basic, or neutral), and additive concentration on the extraction efficiency are examined. The extraction recoveries of lovastatin from MEVACOR tablets are shown to be highly dependent on meth...