A comparative study was carried out for an alloy of Al50(Ni75Mo25)50 processed by two different high energy ball mills. A SPEX and Simoloyer mill were used. The milled products were characterized using X-Ray Diffraction and Scanning Electron Microscopy. A different morphology and microstructural evolution were found with each mill used. It was evident that prolonged milling time induced the for...

We demonstrate here using a disulfide system the first example of reversible, selective, and quantitative transformation between three crystalline polymorphs by ball mill grinding.

Natural Akermanite (NAM) has been successfully prepared by a modified sol-gel method. Optimization in calcination temperature and mechanical ball milling resulted in a pure and nano-sized powder which characterized by means of scanning electron microscopy (SEM), X-ray diffraction (XRD), transmission electron microscopy (TEM) and Fourier transform infrared Spectroscopy (FT–IR). Calcium nitrate, ...

In this research, CuO spherical-like nanoparticles were synthesized using the planetary ball mill method. The structure, particle size and morphology of the resulting CuO nanoparticles were characterized by XRD (X-ray diffraction), SEM (scanning electron microscopy) and SAXS (small-angle X-ray scattering) methods. The results of this investigation showed ...

Mill load (ML) estimation plays a major role in improving the grinding production rate (GPR) and the product quality of the grinding process. The ML parameters, such as mineral to ball volume ratio (MBVR), pulp density (PD) and charge volume ratio (CVR), reflect the load inside the ball mill accurately. The relative amplitudes of the high-dimensional frequency spectrum of shell vibration signal...

In thepresentwork,we investigate the destruction efficiency of hexachlorobenzene (HCB) by milling with various reagents in a planetary ball mill under different milling conditions. Under the same conditions of mill rotary rate and charge ratio, the mixture of magnesium powder and aluminum oxide (Mg/Al2O3) was found best in promoting the destruction of HCB, which can be completed destroyed after...

The impact of attrition ball-mill pretreatment on food waste particle size, soluble chemical oxygen demand (SCOD), biochemical methane potential, and microbial community during anaerobic digestion was investigated based milling speed time. uniformity size improved with increasing SCOD the pretreated samples increased to 4%, 7%, 17% at speeds 150, 225, 300 rpm, respectively, compared control. Mi...

Large macrocycles containing imine and borasiloxane links are obtained in polycondensation reactions of 4-formylbenzeneboronic acid, t-Bu(2)Si(OH)(2), and diamines. The multicomponent reactions can be performed in solution or--advantageously--by mechanochemical syntheses in a ball mill.

the equations governing the motion of steel balls and their impact onto shell liners in industrial semi-autogenous grinding (sag) mills are derived in full details by the authors and are used in order to determine the effective design variables for optimizing the working conditions of the mill and to avoid severe impacts which lead to the breakage of sag mill shell liners. these design variable...

Michaelis-Arbuzov reactions of S-aryl disulfide derivatives of 3'-thiothymidine or 5'-thioadenosine with tris(trimethylsilyl) phosphite proceeded in high yields to the corresponding phosphorothiolate monoesters. Subsequent hydrolytic desilylation and phosphate coupling were effected in one-pot using liquid-assisted grinding in a vibration ball mill. Novel 3',5'- and 5',5'-pyrophosphorothiolate-...