are needed. Since the analysis depth depends on the accelerating voltage of the electron beam, the application of low accelerating voltages limits the characteristic-X-ray generation region to a minute region near the specimen surface. However, the energies of the X-rays are less than those of the accelerated electrons; this causes a new problem: the use of analytical X-ray lines is limited. Th...

limn2o4 spinel cathode materials have been successfully synthesized by solid-state reaction. surface of these particles were modified by nanostructured lifepo4 via sol gel dip coating method. synthesized products were characterized by thermally analyzed by thermogravimetric and differential thermal analysis(tg/dta), x-ray diffraction (xrd), scanning electron microscopy (sem), and energy dispers...

the catalytic oxidation of toluene over copper oxide supported on natural diatomite was investigated. the catalyst was prepared by the wet impregnation method and characterized by using the brunauer emmett teller (bet), field emission scanning electron microscopy (fesem), x-ray diffraction (xrd), x-ray fluorescence (xrf) and temperature-programmed reduction (tpr) analysis. the highest catalytic ...

in current work, cds/black carbon nanocomposites were successfully synthesized with the aid of chestnut and cadmium nitrate as the starting reagents. besides, the effects of preparation parameters such as reaction time, and precursor concentration on the morphology of products and removal of heavy metals (hg+2, pb+2) were studied by scanning electron microscopy images and batch adsorption mode....

The aim of this research is to investigate different X-ray based quantitative phase analysis methods for determination of cristobalite phase content in ceramic cores. For this purpose, four popular routes including peak absolute intensity method, relative intensity ratio method, direct or calibration method and internal standard (or Alexander-Klug) method have been chosen. Some control samples ...

This paper presents a systematic study of the surface chemistry, porous texture and adsorptive characteristics of prepared new activated carbon using Persian mesquite grain. Several techniques and methodologies such as, proximate analysis, N2 adsorption–desorption isotherms, scanning electron microscope (SEM), Fourier transform infrared spectroscopy(FT-IR), X-ray Diffraction (XRD), X-ray photoe...

Mn doped ZnO nanocrystals were prepared by co-precipitation route sintered at 450 °C temperature. XRD results indicate that the samples having hexagonal (wurtzite) structure. From X-ray data it is found that the lattice parameters increase with increasing Mn concentration. The X-ray density decreases with increasing Mn concentration of Zn 1-x Mnx O nanocrystals. It indicates that the Mn...

In this research we report synthesis of new Barium- Cobalt precursor complex with 2,6- pyridine dicarboxylic acid (dipic).Thecomplex[Ba(H2O)6][Co(dipic)2[(1)has been characterized using spectral methods (FT-IR, UV–Vis),elemental analysis and Cyclic voltammetric (CV) method. Also in this study we report thermal decomposition of inorganic precursor complex of (1).Characterization of the binary ox...