نتایج جستجو برای: uv hplc apci ms

تعداد نتایج: 217767  

Journal: :Journal of chromatography. A 2005
David R Rudell James P Mattheis John K Fellman

A method was developed for extracting, identifying, and quantifying diphenylamine (DPA) derivatives in the peel of DPA-treated apples using gradient reversed-phase liquid chromatography with ultraviolet-visible absorption and atmospheric pressure chemical ionization detection (LC-UV-vis-APCI-MS). Compounds routinely analyzed using this method included hydroxylated, nitrosated, nitrated, and met...

Journal: :Horticulturae 2021

Carotenoids are naturally occurring fat-soluble pigments found in many organisms. Because of their extensively conjugated carbon–carbon double bond system, carotenoids potent antioxidants. Although the most abundant carotenoid and best singlet oxygen quencher red tomatoes is lycopene, profiles may vary between genotypes. The objective this work was to perform profile indentification using HPLC-...

2011

The power of traditional high-performance liquid chromatography with UV detection (HPLC-UV, DAD) can be readily extended by simply coupling a mass spectrometer (MS) to an existing system. In the early years of liquid chromatographic mass spectrometry (LC-MS), this coupling was considered exotic and complex. After more than 15 years of refinement, LC-MS systems are robust and easy to use, and pr...

2016
A.P. Topolyan M.A. Belyaeva E.E. Bykov P.V. Coodan E.A. Rogozhin D.A. Strizhevskaya O.M. Ivanova A.V. Ustinov I.V. Mikhura I.A. Prokhorenko V.A. Korshun A.A. Formanovsky

Detection of aminoglycoside antibiotics by MS or HPLC is complicated, because a) carbohydrate molecules have low ionization ability in comparison with other organic molecules (particularly in MALDI-MS), and b) the lack of aromatics and/or amide bonds in the molecules makes common HPLC UV-detectors useless. Here, we report on the application of a previously developed method for amine derivatizat...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2009
Issey Osaka Arifumi Yoshimoto Kazuyoshi Nozaki Hiroshi Moriwaki Hideya Kawasaki Ryuichi Arakawa

The simultaneous LC/MS analyses of hexachlorobenzene (HCB) and pentachlorophenol (PCP), two dioxin precursors were studied by both atmospheric pressure chemical ionization (APCI) and atmospheric pressure photoionization mass spectrometry (APPI/MS). The optimum LC/MS conditions of the simultaneous analysis were determined for these two compounds with different polarity. Ionization by APPI was fo...

Journal: :Rapid communications in mass spectrometry : RCM 1998
W C Byrdwell

Analysis of phospholipids was performed using a liquid chromatographic separation with two mass spectrometers in parallel providing electrospray ionization (ESI) and atmospheric pressure chemical ionization (APCI) data simultaneously from a triple quadrupole instrument and a single quadrupole instrument, respectively. The output from UV-Vis and evaporative light scattering detectors were also a...

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